Novel Benzylidenehydrazide-1,2,3-Triazole Conjugates as Antitubercular Agents: Synthesis and Molecular Docking.


Journal

Mini reviews in medicinal chemistry
ISSN: 1875-5607
Titre abrégé: Mini Rev Med Chem
Pays: Netherlands
ID NLM: 101094212

Informations de publication

Date de publication:
2019
Historique:
received: 06 02 2017
revised: 24 10 2017
accepted: 13 11 2017
pubmed: 19 7 2018
medline: 2 11 2019
entrez: 19 7 2018
Statut: ppublish

Résumé

Novel 1,2,3-triazole based benzylidenehydrazide derivatives were synthesized and evaluated for antitubercular activity against Mycobacterium tuberculosis (MTB) H37Ra, M. bovis BCG and cytotoxic activity. Most of the derivatives exhibited promising in vitro potency against MTB characterized by lower MIC values. Among all the synthesized derivatives, compound 6a and 6j were the most active against active and dormant MTB H37Ra, respectively. Compound 6d was significantly active against dormant and active M. bovis BCG. The structure activity relationship has been explored on the basis of anti-tubercular activity data. The active compounds were also tested against THP-1, A549 and Panc-1 cell lines and showed no significant cytotoxicity. Further, the synthesized compounds were found to have potential antioxidant with IC50 range = 11.19-56.64 µg/mL. The molecular docking study of synthesized compounds was performed against DprE1 enzyme of MTB to understand the binding interactions. Furthermore, synthesized compounds were also analysed for ADME properties and the potency of compounds indicated that, this series can be considered as a starting point for the developement of novel and more potent anti-tubercular agents in future.

Sections du résumé

BACKGROUND & OBJECTIVE OBJECTIVE
Novel 1,2,3-triazole based benzylidenehydrazide derivatives were synthesized and evaluated for antitubercular activity against Mycobacterium tuberculosis (MTB) H37Ra, M. bovis BCG and cytotoxic activity. Most of the derivatives exhibited promising in vitro potency against MTB characterized by lower MIC values.
METHODS METHODS
Among all the synthesized derivatives, compound 6a and 6j were the most active against active and dormant MTB H37Ra, respectively. Compound 6d was significantly active against dormant and active M. bovis BCG.
RESULTS RESULTS
The structure activity relationship has been explored on the basis of anti-tubercular activity data. The active compounds were also tested against THP-1, A549 and Panc-1 cell lines and showed no significant cytotoxicity. Further, the synthesized compounds were found to have potential antioxidant with IC50 range = 11.19-56.64 µg/mL. The molecular docking study of synthesized compounds was performed against DprE1 enzyme of MTB to understand the binding interactions.
CONCLUSION CONCLUSIONS
Furthermore, synthesized compounds were also analysed for ADME properties and the potency of compounds indicated that, this series can be considered as a starting point for the developement of novel and more potent anti-tubercular agents in future.

Identifiants

pubmed: 30019644
pii: MRMC-EPUB-91794
doi: 10.2174/1389557518666180718124858
doi:

Substances chimiques

Antineoplastic Agents 0
Antioxidants 0
Antitubercular Agents 0
Benzylidene Compounds 0
Biphenyl Compounds 0
Picrates 0
Triazoles 0
1,1-diphenyl-2-picrylhydrazyl DFD3H4VGDH

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

1178-1194

Informations de copyright

Copyright© Bentham Science Publishers; For any queries, please email at epub@benthamscience.net.

Auteurs

Mubarak H Shaikh (MH)

Department of Chemistry, Dr. Babasaheb Ambedkar Marathwada University, Aurangabad, 431 004, India.

Dnyaneshwar D Subhedar (DD)

Department of Chemistry, Dr. Babasaheb Ambedkar Marathwada University, Aurangabad, 431 004, India.

Laxman Nawale (L)

Combi Chem-Bio Resource Center, CSIR-National Chemical Laboratory, Pune 411 008, India.

Dhiman Sarkar (D)

Combi Chem-Bio Resource Center, CSIR-National Chemical Laboratory, Pune 411 008, India.

Firoz A Kalam Khan (FAK)

Oriental College of Pharmacy, Sanpada (West), Navi Mumbai 400 705, MS, India.

Jaiprakash N Sangshetti (JN)

Dr. Rafiq Zakaria Campus, Y.B. Chavan College of Pharmacy, Aurangabad 431 001, India.

Bapurao B Shingate (BB)

Department of Chemistry, Dr. Babasaheb Ambedkar Marathwada University, Aurangabad, 431 004, India.

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Classifications MeSH