Asymmetric synthesis and biological evaluation of imidazole- and oxazole-containing synthetic lipoxin A


Journal

European journal of medicinal chemistry
ISSN: 1768-3254
Titre abrégé: Eur J Med Chem
Pays: France
ID NLM: 0420510

Informations de publication

Date de publication:
15 Jan 2019
Historique:
received: 27 07 2018
revised: 02 10 2018
accepted: 19 10 2018
pubmed: 13 11 2018
medline: 5 2 2019
entrez: 13 11 2018
Statut: ppublish

Résumé

Lipoxins (LXs) are endogenously generated eicosanoids with potent bio-actions consistent with attenuation of inflammation. The costly synthesis and metabolic instability of LXs may limit their therapeutic potential. Here we report the synthesis and characterization of novel imidazole-/oxazole-containing synthetic-LX-mimetics (sLXms). The key steps of asymmetric synthesis of putative sLXms include a Suzuki reaction and an asymmetric ketone reduction. The effect of the novel compounds on inflammatory responses was assessed using a human monocyte cell line stably expressing a Nuclear Factor Kappa B (NFkB) reporter gene, by investigating downstream cytokine secretion. The potential interaction of the imidazoles/oxazoles with the molecular target of LXs, i.e. G-protein coupled receptor (GPCR) Formyl Peptide Receptor 2 (ALX/FPR2) was investigated using a cell system where ALX/FPR2 is coupled to the Gα

Identifiants

pubmed: 30419493
pii: S0223-5234(18)30919-X
doi: 10.1016/j.ejmech.2018.10.049
pii:
doi:

Substances chimiques

Imidazoles 0
Lipoxins 0
NF-kappa B 0
Oxazoles 0
Receptors, Formyl Peptide 0
formyl peptide receptor 2, mouse 0
lipoxin A4 0
imidazole 7GBN705NH1

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

80-108

Informations de copyright

Copyright © 2018 Elsevier Masson SAS. All rights reserved.

Auteurs

Monica de Gaetano (M)

School of Medicine, Diabetes Complication Research Centre, UCD Conway Institute, University College Dublin, Belfield, Dublin 4, Ireland.

Eibhlín Butler (E)

Centre for Synthesis and Chemical Biology, School of Chemistry, UCD Conway Institute, University College Dublin, Belfield, Dublin 4, Ireland.

Kevin Gahan (K)

Centre for Synthesis and Chemical Biology, School of Chemistry, UCD Conway Institute, University College Dublin, Belfield, Dublin 4, Ireland.

Andrea Zanetti (A)

Centre for Synthesis and Chemical Biology, School of Chemistry, UCD Conway Institute, University College Dublin, Belfield, Dublin 4, Ireland.

Mariam Marai (M)

School of Medicine, Diabetes Complication Research Centre, UCD Conway Institute, University College Dublin, Belfield, Dublin 4, Ireland.

Jianmin Chen (J)

William Harvey Research Institute, Queen Mary University London, London, UK.

Antonino Cacace (A)

School of Medicine, Diabetes Complication Research Centre, UCD Conway Institute, University College Dublin, Belfield, Dublin 4, Ireland.

Emily Hams (E)

Trinity Biomedical Sciences Institute, Trinity College Dublin, Dublin 2, Ireland.

Catherine Maingot (C)

School of Biotechnology, Dublin City University, Glasnevin, Dublin 9, Ireland.

Alisha McLoughlin (A)

School of Biotechnology, Dublin City University, Glasnevin, Dublin 9, Ireland.

Eoin Brennan (E)

School of Medicine, Diabetes Complication Research Centre, UCD Conway Institute, University College Dublin, Belfield, Dublin 4, Ireland.

Xavier Leroy (X)

Actelion Pharmaceuticals Ltd, Gewerbestrasse 16, 4123, Allschwil, Switzerland.

Christine E Loscher (CE)

School of Biotechnology, Dublin City University, Glasnevin, Dublin 9, Ireland.

Padraic Fallon (P)

Trinity Biomedical Sciences Institute, Trinity College Dublin, Dublin 2, Ireland.

Mauro Perretti (M)

William Harvey Research Institute, Queen Mary University London, London, UK.

Catherine Godson (C)

School of Medicine, Diabetes Complication Research Centre, UCD Conway Institute, University College Dublin, Belfield, Dublin 4, Ireland.

Patrick J Guiry (PJ)

Centre for Synthesis and Chemical Biology, School of Chemistry, UCD Conway Institute, University College Dublin, Belfield, Dublin 4, Ireland. Electronic address: p.guiry@ucd.ie.

Articles similaires

[Redispensing of expensive oral anticancer medicines: a practical application].

Lisanne N van Merendonk, Kübra Akgöl, Bastiaan Nuijen
1.00
Humans Antineoplastic Agents Administration, Oral Drug Costs Counterfeit Drugs

Smoking Cessation and Incident Cardiovascular Disease.

Jun Hwan Cho, Seung Yong Shin, Hoseob Kim et al.
1.00
Humans Male Smoking Cessation Cardiovascular Diseases Female
Humans United States Aged Cross-Sectional Studies Medicare Part C
1.00
Humans Yoga Low Back Pain Female Male

Classifications MeSH