Synthesis, Urease Inhibition and Molecular Modelling Studies of Novel Derivatives of the Naturally Occurring β-Amyrenone.

Docking Helicobacter pylori Olean-12-en-3-one derivatives Urease inhibition

Journal

Natural products and bioprospecting
ISSN: 2192-2195
Titre abrégé: Nat Prod Bioprospect
Pays: Germany
ID NLM: 101577734

Informations de publication

Date de publication:
Jan 2019
Historique:
received: 15 10 2018
accepted: 13 11 2018
pubmed: 30 11 2018
medline: 30 11 2018
entrez: 30 11 2018
Statut: ppublish

Résumé

Urease enzyme (UE) has been reported to be a potent virulence factor for Helicobacter pylori (HP) bacteria indicated to be responsible for various gastrointestinal diseases. Therefore, the spread of HP, currently regarded by the World Health Organization as a class 1 carcinogen, could be better controlled by targeting UE. It is in this line that we have synthesized three new derivatives (2-4) of the naturally occurring olean-12-en-3-one (1), which was previously isolated from the figs of Ficus vallis-choudae Delile (Moraceae). Among the synthesized compounds, 3 and 4 contain an indole moiety. Their structures were unambiguously assigned by spectroscopic and spectrometric techniques (1D-NMR, 2D-NMR and MS). The starting material and the synthesized compounds were screened for UE inhibition activity, and showed significant activities with IC

Identifiants

pubmed: 30488317
doi: 10.1007/s13659-018-0193-7
pii: 10.1007/s13659-018-0193-7
pmc: PMC6328428
doi:

Types de publication

Journal Article

Langues

eng

Pagination

49-59

Subventions

Organisme : ICCBS-TWAS Postdoctoral Fellowship
ID : 3240280476

Références

J Ethnopharmacol. 1999 Sep;66(3):289-93
pubmed: 10473175
Science. 2002 Nov 29;298(5599):1788-90
pubmed: 12459589
J Med Chem. 2004 Mar 25;47(7):1739-49
pubmed: 15027865
J Med Chem. 2004 Mar 25;47(7):1750-9
pubmed: 15027866
J Comput Chem. 2005 Dec;26(16):1752-80
pubmed: 16211539
Clin Microbiol Rev. 2006 Jul;19(3):449-90
pubmed: 16847081
Best Pract Res Clin Gastroenterol. 2007;21(2):205-14
pubmed: 17382273
J Med Chem. 2010 Apr 8;53(7):2719-40
pubmed: 20131845
J Chem Inf Model. 2010 Apr 26;50(4):534-46
pubmed: 20373803
J Biol Chem. 2011 Dec 16;286(50):43241-9
pubmed: 22013070
J Comput Aided Mol Des. 2013 Mar;27(3):221-34
pubmed: 23579614
PLoS Biol. 2013 Oct;11(10):e1001678
pubmed: 24115911
J Biol Chem. 2014 Feb 14;289(7):3828-41
pubmed: 24338018
Biomark Res. 2017 Jul 11;5:23
pubmed: 28702193
Protein Sci. 2018 Jan;27(1):316-330
pubmed: 29067736
Fitoterapia. 2018 Jan;124:73-79
pubmed: 29074226
Phytochemistry. 2018 Jan;145:68-76
pubmed: 29101786
Z Naturforsch C. 2018 Sep 25;73(9-10):335-344
pubmed: 29320368
Fitoterapia. 2018 Mar;125:155-160
pubmed: 29355750
Infect Immun. 1994 Sep;62(9):3604-7
pubmed: 8063376
FEMS Microbiol Lett. 1996 Jul 15;141(1):71-6
pubmed: 8764511

Auteurs

Jean J K Bankeu (JJK)

Department of Chemistry, Faculty of Science, The University of Bamenda, P.O. Box 39, Bambili, Cameroon. bk_jeanjules@yahoo.fr.
International Center for Chemical and Biological Sciences, University of Karachi, Karachi, 75270, Pakistan. bk_jeanjules@yahoo.fr.

Hira Sattar (H)

International Center for Chemical and Biological Sciences, University of Karachi, Karachi, 75270, Pakistan.

Yannick S F Fongang (YSF)

International Center for Chemical and Biological Sciences, University of Karachi, Karachi, 75270, Pakistan.
Department of Chemistry, Higher Teacher Training College, University of Maroua, P.O. Box 55, Maroua, Cameroon.

Syeda W Muhammadi (SW)

International Center for Chemical and Biological Sciences, University of Karachi, Karachi, 75270, Pakistan.

Conrad V Simoben (CV)

Department of Pharmaceutical Chemistry, Martin-Luther University of Halle-Wittenberg, Wolfgang-Langenbeck-Str. 4, 06120, Halle (Saale), Germany.

Fidele Ntie-Kang (F)

Department of Pharmaceutical Chemistry, Martin-Luther University of Halle-Wittenberg, Wolfgang-Langenbeck-Str. 4, 06120, Halle (Saale), Germany. ntiekfidele@gmail.com.
Department of Chemistry, Faculty of Science, University of Buea, P. O. Box 63, Buea, Cameroon. ntiekfidele@gmail.com.

Guy R T Feuya (GRT)

Department of Chemistry, Faculty of Science, Scientific and Technical University of Masuku, Box 943, Franceville, Gabon.

Marthe A T Tchuenmogne (MAT)

Department of Chemistry, Faculty of Science, University of Yaoundé I, P.O. Box 812, Yaoundé, Cameroon.

Mehreen Lateef (M)

Multi-Disciplinary Research Laboratory (MDRL), Bahria University Medical and Dental College, Bahria University, Karachi, Pakistan.

Bruno N Lenta (BN)

Department of Chemistry, Higher Teacher Training College, University of Yaoundé I, P.O. Box 47, Yaoundé, Cameroon. lentabruno@yahoo.fr.

Muhammad S Ali (MS)

International Center for Chemical and Biological Sciences, University of Karachi, Karachi, 75270, Pakistan.

Augustin S Ngouela (AS)

Department of Chemistry, Faculty of Science, University of Yaoundé I, P.O. Box 812, Yaoundé, Cameroon.

Classifications MeSH