A Highly Effective Route to Si-O-Si Moieties through O-Silylation of Silanols and Polyhedral Oligomeric Silsesquioxane Silanols with Disilazanes.

catalyst-free chlorine-free disilazanes siloxanes silsesquioxanes

Journal

ChemSusChem
ISSN: 1864-564X
Titre abrégé: ChemSusChem
Pays: Germany
ID NLM: 101319536

Informations de publication

Date de publication:
07 Mar 2019
Historique:
received: 27 11 2018
pubmed: 12 12 2018
medline: 12 12 2018
entrez: 12 12 2018
Statut: ppublish

Résumé

A simple and highly practical catalyst-free O-silylation of silanols with commercially available disilazanes has been developed under mild conditions. In the case of polyhedral oligomeric silsesquioxane (POSS) silanols and some other silanols, it was necessary to use catalytic amounts of inexpensive Bi(OTf)

Identifiants

pubmed: 30536641
doi: 10.1002/cssc.201802757
doi:

Types de publication

Journal Article

Langues

eng

Pagination

1043-1048

Subventions

Organisme : Narodowe Centrum Nauki
ID : UMO-2015/19/B/ST5/00240

Informations de copyright

© 2019 Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim.

Auteurs

Krzysztof Kuciński (K)

Faculty of Chemistry, Adam Mickiewicz University in Poznań, Umultowska 89b, 61-614, Poznań, Poland.

Grzegorz Hreczycho (G)

Faculty of Chemistry, Adam Mickiewicz University in Poznań, Umultowska 89b, 61-614, Poznań, Poland.

Classifications MeSH