Synthesis and Fabrication of Surface-Active Microparticles Using a Membrane Emulsion Technique and Conjugation of Model Protein via Strain-Promoted Azide-Alkyne Click Chemistry in Physiological Conditions.


Journal

Bioconjugate chemistry
ISSN: 1520-4812
Titre abrégé: Bioconjug Chem
Pays: United States
ID NLM: 9010319

Informations de publication

Date de publication:
20 03 2019
Historique:
pubmed: 8 2 2019
medline: 30 11 2019
entrez: 8 2 2019
Statut: ppublish

Résumé

The rapid surface immobilization of protein on monodispersed polyester microcarriers is reported. A model protein, functionalized with a dibenzocyclooctyne core, immobilizes on the surface of azide-terminal polycaprolactone microcarriers within 10 min compared to 12 h for other conjugation techniques, and it is conducted in physiological conditions and in the absence of coupling reagents.

Identifiants

pubmed: 30730698
doi: 10.1021/acs.bioconjchem.8b00868
doi:

Substances chimiques

Alkynes 0
Azides 0
Cyclooctanes 0
Emulsions 0
Immobilized Proteins 0
Polyesters 0
polycaprolactone 24980-41-4
Serum Albumin, Human ZIF514RVZR

Types de publication

Journal Article Research Support, Non-U.S. Gov't

Langues

eng

Sous-ensembles de citation

IM

Pagination

531-535

Auteurs

Grace Walden (G)

School of Pharmacy , University of East Anglia , Norwich NR4 7TJ , United Kingdom.

Xin Liao (X)

School of Pharmacy , University of East Anglia , Norwich NR4 7TJ , United Kingdom.

Graham Riley (G)

School of Biological Sciences , University of East Anglia , Norwich NR4 7TJ , United Kingdom.

Simon Donell (S)

Norwich Medical School , University of East Anglia , Norwich NR4 7TJ , United Kingdom.

Michael J Raxworthy (MJ)

Neotherix Limited , York YO1 7PR , United Kingdom.

Aram Saeed (A)

School of Pharmacy , University of East Anglia , Norwich NR4 7TJ , United Kingdom.

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Classifications MeSH