Clay-Na as a sorbent for the extraction of anti-inflammatory compounds in water samples.


Journal

Journal of separation science
ISSN: 1615-9314
Titre abrégé: J Sep Sci
Pays: Germany
ID NLM: 101088554

Informations de publication

Date de publication:
May 2019
Historique:
received: 03 12 2018
revised: 31 01 2019
accepted: 20 02 2019
pubmed: 7 3 2019
medline: 23 7 2019
entrez: 7 3 2019
Statut: ppublish

Résumé

In this work, clay-Na particles are used as the adsorbent for the solid-phase extraction of acidic compounds. The novel sorbent under study is based on high-specific surface area, cation-exchange capacity designed specifically to offer ion-exchange properties with the goal being to selectively extract a group of acidic compounds. The effects of the extraction parameters including extraction elution solvent, sample volume and pH. In optimum conditions, the repeatability for one fiber (n = 3), expressed as % relative standard deviation, was between 0.3 and 4.3% for the acid compounds. The detection limits for the studied acidic compounds were between 0.1-0.6 μg/L. The developed method offers the advantages of being simple to use and having a low cost of equipment.

Identifiants

pubmed: 30839163
doi: 10.1002/jssc.201801251
doi:

Substances chimiques

Anti-Inflammatory Agents 0
Water Pollutants, Chemical 0
Sodium 9NEZ333N27
Clay T1FAD4SS2M

Types de publication

Evaluation Study Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

1710-1716

Informations de copyright

© 2019 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

Auteurs

Hassen Khazri (H)

Laboratory of Materials, Processing and Analysis (LMTA), National Institute of Research and Physical-Chemical Analysis (INRAP), Biotechpole Sidi Thabet, Ariana, Tunisia.
Laboratory of Application Chemistry to the Resources and Natural Substances and the Environment (LACReSNE), Faculty of Science of Bizerte, Zarzouna, Bizerte, Tunisia.

Ibtissem Ghorbel-Abid (I)

Laboratory of Materials, Processing and Analysis (LMTA), National Institute of Research and Physical-Chemical Analysis (INRAP), Biotechpole Sidi Thabet, Ariana, Tunisia.
Laboratory of Application Chemistry to the Resources and Natural Substances and the Environment (LACReSNE), Faculty of Science of Bizerte, Zarzouna, Bizerte, Tunisia.

Sihem Ben Hassine (S)

Joint Research Laboratory, Department of Life Sciences, Faculty of Science of Bizerte, University of Carthage, Zarzouna, Bizerte, Tunisia.

Sylvie Chevolleau (S)

Toxalim (Research Centre in Food Toxicology), INRA, ENVT, INP-Purpan, Université de Toulouse, Toulouse, France.
Axiom platform, MetaToul-MetaboHUB, National Infrastructure for Metabolomics and Fluxomics, Toulouse, France.

Laurent Debrauwer (L)

Toxalim (Research Centre in Food Toxicology), INRA, ENVT, INP-Purpan, Université de Toulouse, Toulouse, France.
Axiom platform, MetaToul-MetaboHUB, National Infrastructure for Metabolomics and Fluxomics, Toulouse, France.

Rafik Kalfat (R)

Laboratory of Materials, Processing and Analysis (LMTA), National Institute of Research and Physical-Chemical Analysis (INRAP), Biotechpole Sidi Thabet, Ariana, Tunisia.

Malika Trabelsi-Ayadi (M)

Laboratory of Application Chemistry to the Resources and Natural Substances and the Environment (LACReSNE), Faculty of Science of Bizerte, Zarzouna, Bizerte, Tunisia.

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Classifications MeSH