Monolayer black phosphorus by sequential wet-chemical surface oxidation.


Journal

RSC advances
ISSN: 2046-2069
Titre abrégé: RSC Adv
Pays: England
ID NLM: 101581657

Informations de publication

Date de publication:
25 Jan 2019
Historique:
received: 01 11 2018
accepted: 17 01 2019
entrez: 12 3 2019
pubmed: 12 3 2019
medline: 12 3 2019
Statut: epublish

Résumé

We report a straightforward chemical methodology for controlling the thickness of black phosphorus flakes down to the monolayer limit by layer-by-layer oxidation and thinning, using water as solubilizing agent. Moreover, the oxidation process can be stopped at will by two different passivation procedures, namely the non-covalent functionalization with perylene diimide chromophores, which prevents the photooxidation, or by using a protective ionic liquid layer. The obtained flakes preserve their electronic properties as demonstrated by fabricating a BP field-effect transistor (FET). This work paves the way for the preparation of BP devices with controlled thickness.

Identifiants

pubmed: 30854196
doi: 10.1039/c8ra09069f
pii: c8ra09069f
pmc: PMC6369675
doi:

Types de publication

Journal Article

Langues

eng

Pagination

3570-3576

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Auteurs

Stefan Wild (S)

Department of Chemistry and Pharmacy, Joint Institute of Advanced Materials and Processes (ZMP), Friedrich-Alexander-Universität Erlangen-Nürnberg (FAU), Nikolaus Fiebiger-Strasse 10, 91058 Erlangen, Germany. Email: gonzalo.abellan@fau.de; Email: andreas.hirsch@fau.de.

Vicent Lloret (V)

Department of Chemistry and Pharmacy, Joint Institute of Advanced Materials and Processes (ZMP), Friedrich-Alexander-Universität Erlangen-Nürnberg (FAU), Nikolaus Fiebiger-Strasse 10, 91058 Erlangen, Germany. Email: gonzalo.abellan@fau.de; Email: andreas.hirsch@fau.de.

Victor Vega-Mayoral (V)

CRANN & AMBER Research Centers, School of Physics, Trinity College Dublin, Dublin 2, Ireland.
Department of Complex Matter, Jozef Stefan Institute, Jozef Stefan International Postgraduate School, Jamova 39, 1000 Ljubljana, Slovenia.

Daniele Vella (D)

Department of Complex Matter, Jozef Stefan Institute, Jozef Stefan International Postgraduate School, Jamova 39, 1000 Ljubljana, Slovenia.
Department of Physics, National University of Singapore, 2 Science Drive 3, Singapore 117542, Singapore.

Edurne Nuin (E)

Department of Chemistry and Pharmacy, Joint Institute of Advanced Materials and Processes (ZMP), Friedrich-Alexander-Universität Erlangen-Nürnberg (FAU), Nikolaus Fiebiger-Strasse 10, 91058 Erlangen, Germany. Email: gonzalo.abellan@fau.de; Email: andreas.hirsch@fau.de.
Instituto de Ciencia Molecular (ICMol), Universidad de Valencia, Catedrático José Beltrán 2, 46980, Paterna, Valencia, Spain.

Martin Siebert (M)

Department of Physics, Friedrich-Alexander-Universität Erlangen-Nürnberg (FAU), Staudtstr. 7, 91058 Erlangen, Germany.

Maria Koleśnik-Gray (M)

Department of Physics, Friedrich-Alexander-Universität Erlangen-Nürnberg (FAU), Staudtstr. 7, 91058 Erlangen, Germany.

Mario Löffler (M)

Helmholtz Institute Erlangen-Nürnberg for Renewable Energy (IEK-11), Forschungszentrum Jülich GmbH, Egerlandstraße 3, 91058 Erlangen, Germany.
Department of Chemical and Biological Engineering, Friedrich-Alexander-Universität Erlangen-Nürnberg (FAU), Immerwahrstraße 2a, 91058 Erlangen, Germany.

Karl J J Mayrhofer (KJJ)

Helmholtz Institute Erlangen-Nürnberg for Renewable Energy (IEK-11), Forschungszentrum Jülich GmbH, Egerlandstraße 3, 91058 Erlangen, Germany.
Department of Chemical and Biological Engineering, Friedrich-Alexander-Universität Erlangen-Nürnberg (FAU), Immerwahrstraße 2a, 91058 Erlangen, Germany.

Christoph Gadermaier (C)

Department of Complex Matter, Jozef Stefan Institute, Jozef Stefan International Postgraduate School, Jamova 39, 1000 Ljubljana, Slovenia.
Department of Physics, Politecnico di Milano, Piazza Leonardo da Vinci 32, 20133 Milano, Italy.

Vojislav Krstić (V)

Department of Physics, Friedrich-Alexander-Universität Erlangen-Nürnberg (FAU), Staudtstr. 7, 91058 Erlangen, Germany.

Frank Hauke (F)

Department of Chemistry and Pharmacy, Joint Institute of Advanced Materials and Processes (ZMP), Friedrich-Alexander-Universität Erlangen-Nürnberg (FAU), Nikolaus Fiebiger-Strasse 10, 91058 Erlangen, Germany. Email: gonzalo.abellan@fau.de; Email: andreas.hirsch@fau.de.

Gonzalo Abellán (G)

Department of Chemistry and Pharmacy, Joint Institute of Advanced Materials and Processes (ZMP), Friedrich-Alexander-Universität Erlangen-Nürnberg (FAU), Nikolaus Fiebiger-Strasse 10, 91058 Erlangen, Germany. Email: gonzalo.abellan@fau.de; Email: andreas.hirsch@fau.de.
Instituto de Ciencia Molecular (ICMol), Universidad de Valencia, Catedrático José Beltrán 2, 46980, Paterna, Valencia, Spain.

Andreas Hirsch (A)

Department of Chemistry and Pharmacy, Joint Institute of Advanced Materials and Processes (ZMP), Friedrich-Alexander-Universität Erlangen-Nürnberg (FAU), Nikolaus Fiebiger-Strasse 10, 91058 Erlangen, Germany. Email: gonzalo.abellan@fau.de; Email: andreas.hirsch@fau.de.

Classifications MeSH