Fixed-target serial oscillation crystallography at room temperature.
X-ray crystallography
fixed-target serial oscillation
oscillations
radiation damage
serial crystallography
storage rings
structural biology
structure determination
Journal
IUCrJ
ISSN: 2052-2525
Titre abrégé: IUCrJ
Pays: England
ID NLM: 101623101
Informations de publication
Date de publication:
01 Mar 2019
01 Mar 2019
Historique:
received:
18
11
2018
accepted:
25
01
2019
entrez:
15
3
2019
pubmed:
15
3
2019
medline:
15
3
2019
Statut:
epublish
Résumé
A fixed-target approach to high-throughput room-temperature serial synchrotron crystallography with oscillation is described. Patterned silicon chips with microwells provide high crystal-loading density with an extremely high hit rate. The microfocus, undulator-fed beamline at CHESS, which has compound refractive optics and a fast-framing detector, was built and optimized for this experiment. The high-throughput oscillation method described here collects 1-5° of data per crystal at room temperature with fast (10° s
Identifiants
pubmed: 30867928
doi: 10.1107/S2052252519001453
pii: mf5030
pmc: PMC6400179
doi:
Types de publication
Journal Article
Langues
eng
Pagination
305-316Subventions
Organisme : NIGMS NIH HHS
ID : P41 GM103485
Pays : United States
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