Atypical Lone Pair-π Interaction with Quinone Methides in a Series of Imido-Ferrociphenol Anticancer Drug Candidates.


Journal

Angewandte Chemie (International ed. in English)
ISSN: 1521-3773
Titre abrégé: Angew Chem Int Ed Engl
Pays: Germany
ID NLM: 0370543

Informations de publication

Date de publication:
17 06 2019
Historique:
received: 25 02 2019
revised: 29 03 2019
pubmed: 13 4 2019
medline: 15 9 2020
entrez: 13 4 2019
Statut: ppublish

Résumé

Ferrociphenols, especially those possessing a heterocycle at the terminus of an aliphatic chain, display strong anticancer activity through a novel redox mechanism that generates active metabolites such as quinone methides (QMs). X-ray crystallography and UV/Vis spectroscopy reveal that the specific lone pair (lp)-π interaction between a carbonyl group of the imide and the quinone motif of the QM plays an important role in the exceptional cytotoxic behaviour of their imido-ferrociphenol precursors. This intramolecular lp-π interaction markedly enhanced the stability of the QMs and lowered the pK

Identifiants

pubmed: 30977944
doi: 10.1002/anie.201902456
doi:

Substances chimiques

Antineoplastic Agents 0
Ferrous Compounds 0
Imides 0
Indolequinones 0
ferrociphenol 0
quinone methide 138230-21-4

Types de publication

Journal Article Research Support, Non-U.S. Gov't

Langues

eng

Sous-ensembles de citation

IM

Pagination

8421-8425

Subventions

Organisme : H2020 European Research Council
ID : 648558
Pays : International

Informations de copyright

© 2019 Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim.

Auteurs

Yong Wang (Y)

PSL, Chimie ParisTech, 11 rue Pierre et Marie Curie, F-75005, Paris, France.
Sorbonne Université, UPMC Univ Paris 6, UMR 8232 CNRS, IPCM, place Jussieu, F-75005, Paris, France.

Pascal Pigeon (P)

PSL, Chimie ParisTech, 11 rue Pierre et Marie Curie, F-75005, Paris, France.
Sorbonne Université, UPMC Univ Paris 6, UMR 8232 CNRS, IPCM, place Jussieu, F-75005, Paris, France.

Siden Top (S)

Sorbonne Université, UPMC Univ Paris 6, UMR 8232 CNRS, IPCM, place Jussieu, F-75005, Paris, France.

Juan Sanz García (J)

PSL, Chimie ParisTech, 11 rue Pierre et Marie Curie, F-75005, Paris, France.

Claire Troufflard (C)

Sorbonne Université, UPMC Univ Paris 6, UMR 8232 CNRS, IPCM, place Jussieu, F-75005, Paris, France.

Ilaria Ciofini (I)

PSL, Chimie ParisTech, 11 rue Pierre et Marie Curie, F-75005, Paris, France.

Michael J McGlinchey (MJ)

UCD School of Chemistry, University College Dublin, Belfield, Dublin 4, Ireland.

Gérard Jaouen (G)

PSL, Chimie ParisTech, 11 rue Pierre et Marie Curie, F-75005, Paris, France.
Sorbonne Université, UPMC Univ Paris 6, UMR 8232 CNRS, IPCM, place Jussieu, F-75005, Paris, France.

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Classifications MeSH