Standardization procedures for real-time breath analysis by secondary electrospray ionization high-resolution mass spectrometry.


Journal

Analytical and bioanalytical chemistry
ISSN: 1618-2650
Titre abrégé: Anal Bioanal Chem
Pays: Germany
ID NLM: 101134327

Informations de publication

Date de publication:
Jul 2019
Historique:
received: 03 12 2018
accepted: 06 03 2019
revised: 25 02 2019
pubmed: 17 4 2019
medline: 31 7 2019
entrez: 17 4 2019
Statut: ppublish

Résumé

Despite the attractiveness of breath analysis as a non-invasive means to retrieve relevant metabolic information, its introduction into routine clinical practice remains a challenge. Among all the different analytical techniques available to interrogate exhaled breath, secondary electrospray ionization high-resolution mass spectrometry (SESI-HRMS) offers a number of advantages (e.g., real-time, yet wide, metabolome coverage) that makes it ideal for untargeted and targeted studies. However, so far, SESI-HRMS has relied mostly on lab-built prototypes, making it difficult to standardize breath sampling and subsequent analysis, hence preventing further developments such as multi-center clinical studies. To address this issue, we present here a number of new developments. In particular, we have characterized a new SESI interface featuring real-time readout of critical exhalation parameters such as CO

Identifiants

pubmed: 30989265
doi: 10.1007/s00216-019-01764-8
pii: 10.1007/s00216-019-01764-8
pmc: PMC6611759
doi:

Substances chimiques

Biomarkers 0

Types de publication

Journal Article

Langues

eng

Pagination

4883-4898

Subventions

Organisme : Schweizerischer Nationalfonds zur Förderung der Wissenschaftlichen Forschung
ID : PCEGP3_181300

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Auteurs

Kapil Dev Singh (KD)

University Children's Hospital Basel, University of Basel, Spitalstr. 33, 4056, Basel, Switzerland.
Department of Biomedical Engineering, University of Basel, Gewerbestr. 14, 4123, Allschwil, Switzerland.

Georgi Tancev (G)

University Children's Hospital Basel, University of Basel, Spitalstr. 33, 4056, Basel, Switzerland.
Department of Biomedical Engineering, University of Basel, Gewerbestr. 14, 4123, Allschwil, Switzerland.

Fabienne Decrue (F)

University Children's Hospital Basel, University of Basel, Spitalstr. 33, 4056, Basel, Switzerland.

Jakob Usemann (J)

University Children's Hospital Basel, University of Basel, Spitalstr. 33, 4056, Basel, Switzerland.

Rhea Appenzeller (R)

University Children's Hospital Basel, University of Basel, Spitalstr. 33, 4056, Basel, Switzerland.

Pedro Barreiro (P)

Fossil Ion Technology S.L., Calle la Gitanilla 17, 29004, Malaga, Spain.

Gabriel Jaumà (G)

Fossil Ion Technology S.L., Calle la Gitanilla 17, 29004, Malaga, Spain.

Miriam Macia Santiago (M)

Fossil Ion Technology S.L., Calle la Gitanilla 17, 29004, Malaga, Spain.

Guillermo Vidal de Miguel (G)

Fossil Ion Technology S.L., Calle la Gitanilla 17, 29004, Malaga, Spain.

Urs Frey (U)

University Children's Hospital Basel, University of Basel, Spitalstr. 33, 4056, Basel, Switzerland.
Department of Biomedical Engineering, University of Basel, Gewerbestr. 14, 4123, Allschwil, Switzerland.

Pablo Sinues (P)

University Children's Hospital Basel, University of Basel, Spitalstr. 33, 4056, Basel, Switzerland. pablo.sinues@unibas.ch.
Department of Biomedical Engineering, University of Basel, Gewerbestr. 14, 4123, Allschwil, Switzerland. pablo.sinues@unibas.ch.

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Classifications MeSH