A MOF@COF Composite with Enhanced Uptake through Interfacial Pore Generation.

composite materials covalent-organic frameworks hierarchical porosity interfaces metal-organic frameworks

Journal

Angewandte Chemie (International ed. in English)
ISSN: 1521-3773
Titre abrégé: Angew Chem Int Ed Engl
Pays: Germany
ID NLM: 0370543

Informations de publication

Date de publication:
08 Jul 2019
Historique:
received: 17 04 2019
pubmed: 16 5 2019
medline: 16 5 2019
entrez: 16 5 2019
Statut: ppublish

Résumé

Herein, we describe a new class of porous composites comprising metal-organic framework (MOF) crystals confined in single spherical matrices made of packed covalent-organic framework (COF) nanocrystals. These MOF@COF composites are synthesized through a two-step method of spray-drying and subsequent amorphous (imine-based polymer)-to-crystalline (imine-based COF) transformation. This transformation around the MOF crystals generates micro- and mesopores at the MOF/COF interface that provide far superior porosity compared to that of the constituent MOF and COF components added together. We report that water sorption in these new pores occurs within the same pressure window as in the COF pores. Our new MOF@COF composites, with their additional pores at the MOF/COF interface, should have implications for the development of new composites.

Identifiants

pubmed: 31087600
doi: 10.1002/anie.201904766
doi:

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

9512-9516

Subventions

Organisme : FP7 Ideas: European Research Council
ID : ERC-Co-615954

Informations de copyright

© 2019 Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim.

Auteurs

Luis Garzón-Tovar (L)

Catalan Institute of Nanoscience and Nanotechnology (ICN2), CSIC and BIST, Campus UAB, Bellaterra, 08193, Barcelona, Spain.

Javier Pérez-Carvajal (J)

Catalan Institute of Nanoscience and Nanotechnology (ICN2), CSIC and BIST, Campus UAB, Bellaterra, 08193, Barcelona, Spain.

Amirali Yazdi (A)

Catalan Institute of Nanoscience and Nanotechnology (ICN2), CSIC and BIST, Campus UAB, Bellaterra, 08193, Barcelona, Spain.

Jose Hernández-Muñoz (J)

Departamento de Física Teórica de la Materia Condensada, IFIMAC Condensed Matter Physics Center, Universidad Autónoma de Madrid, 28049, Madrid, Spain.

Pedro Tarazona (P)

Departamento de Física Teórica de la Materia Condensada, IFIMAC Condensed Matter Physics Center, Universidad Autónoma de Madrid, 28049, Madrid, Spain.

Inhar Imaz (I)

Catalan Institute of Nanoscience and Nanotechnology (ICN2), CSIC and BIST, Campus UAB, Bellaterra, 08193, Barcelona, Spain.

Félix Zamora (F)

Departamento de Química Inorgánica and Institute for Advanced Research in Chemical Sciences (IAdChem), Universidad Autónoma de Madrid, 28049, Madrid, Spain.
Instituto Madrileño de Estudios Avanzados en Nanociencia (IMDEA Nanociencia), Cantoblanco, 28049, Madrid, Spain.

Daniel Maspoch (D)

Catalan Institute of Nanoscience and Nanotechnology (ICN2), CSIC and BIST, Campus UAB, Bellaterra, 08193, Barcelona, Spain.
ICREA, Pg. Lluís Companys 23, 08010, Barcelona, Spain.

Classifications MeSH