Structural and Functional Analyses of an Allosteric EYA2 Phosphatase Inhibitor That Has On-Target Effects in Human Lung Cancer Cells.


Journal

Molecular cancer therapeutics
ISSN: 1538-8514
Titre abrégé: Mol Cancer Ther
Pays: United States
ID NLM: 101132535

Informations de publication

Date de publication:
09 2019
Historique:
received: 01 11 2018
revised: 05 05 2019
accepted: 28 06 2019
pubmed: 10 7 2019
medline: 18 6 2020
entrez: 10 7 2019
Statut: ppublish

Résumé

EYA proteins (EYA1-4) are critical developmental transcriptional cofactors that contain an EYA domain (ED) harboring Tyr phosphatase activity. EYA proteins are largely downregulated after embryogenesis but are reexpressed in cancers, and their Tyr phosphatase activity plays an important role in the DNA damage response and tumor progression. We previously identified a class of small-molecule allosteric inhibitors that specifically inhibit the Tyr phosphatase activity of EYA2. Herein, we determined the crystal structure of the EYA2 ED in complex with NCGC00249987 (a representative compound in this class), revealing that it binds to an induced pocket distant from the active site. NCGC00249987 binding leads to a conformational change of the active site that is unfavorable for Mg

Identifiants

pubmed: 31285279
pii: 1535-7163.MCT-18-1239
doi: 10.1158/1535-7163.MCT-18-1239
pmc: PMC6726557
mid: NIHMS1038649
doi:

Substances chimiques

Enzyme Inhibitors 0
Intracellular Signaling Peptides and Proteins 0
Nuclear Proteins 0
Small Molecule Libraries 0
protein phosphatase inhibitor-1 0
EYA2 protein, human EC 3.1.3.48
Protein Tyrosine Phosphatases EC 3.1.3.48

Types de publication

Journal Article Research Support, N.I.H., Extramural Research Support, Non-U.S. Gov't

Langues

eng

Sous-ensembles de citation

IM

Pagination

1484-1496

Subventions

Organisme : NCI NIH HHS
ID : F99 CA234940
Pays : United States
Organisme : NCI NIH HHS
ID : K00 CA234940
Pays : United States
Organisme : NIDA NIH HHS
ID : R03 DA030559
Pays : United States
Organisme : NCI NIH HHS
ID : R41 CA180347
Pays : United States
Organisme : NINDS NIH HHS
ID : R01 NS108396
Pays : United States

Informations de copyright

©2019 American Association for Cancer Research.

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Auteurs

Jothi Anantharajan (J)

Experimental Drug Discovery Centre, A*STAR, Singapore, Singapore.

Hengbo Zhou (H)

Department of Pharmacology, University of Colorado Denver Anschutz Medical Campus, Aurora, Colorado.

Lingdi Zhang (L)

Department of Biochemistry and Molecular Genetics, University of Colorado Denver Anschutz Medical Campus, Aurora, Colorado.

Taylor Hotz (T)

Department of Pharmacology, University of Colorado Denver Anschutz Medical Campus, Aurora, Colorado.

Melanie Y Vincent (MY)

Department of Pharmacology, University of Colorado Denver Anschutz Medical Campus, Aurora, Colorado.

Melanie A Blevins (MA)

Department of Biochemistry and Molecular Genetics, University of Colorado Denver Anschutz Medical Campus, Aurora, Colorado.

Anna E Jansson (AE)

Experimental Drug Discovery Centre, A*STAR, Singapore, Singapore.

John Wee Liang Kuan (JWL)

Experimental Drug Discovery Centre, A*STAR, Singapore, Singapore.

Elizabeth Yihui Ng (EY)

Experimental Drug Discovery Centre, A*STAR, Singapore, Singapore.

Yee Khoon Yeo (YK)

Experimental Drug Discovery Centre, A*STAR, Singapore, Singapore.

Nithya Baburajendran (N)

Experimental Drug Discovery Centre, A*STAR, Singapore, Singapore.

Grace Lin (G)

Experimental Drug Discovery Centre, A*STAR, Singapore, Singapore.

Alvin W Hung (AW)

Experimental Drug Discovery Centre, A*STAR, Singapore, Singapore.

Joma Joy (J)

Experimental Drug Discovery Centre, A*STAR, Singapore, Singapore.

Samarjit Patnaik (S)

National Center for Advancing Translational Sciences, National Institutes of Health, Bethesda, Maryland.

Juan Marugan (J)

National Center for Advancing Translational Sciences, National Institutes of Health, Bethesda, Maryland.

Pratyaydipta Rudra (P)

Department of Biostatistics and Informatics, University of Colorado Anschutz Medical Campus, Aurora, Colorado.

Debashis Ghosh (D)

Department of Biostatistics and Informatics, University of Colorado Anschutz Medical Campus, Aurora, Colorado.

Jeffrey Hill (J)

Experimental Drug Discovery Centre, A*STAR, Singapore, Singapore. heide.ford@cuanschutz.edu jhill@eddc.a-star.edu.sg thkeller@eddc.a-star.edu.sg rui.zhao@cuanschutz.edu cbkang@eddc.a-star.edu.sg.

Thomas H Keller (TH)

Experimental Drug Discovery Centre, A*STAR, Singapore, Singapore. heide.ford@cuanschutz.edu jhill@eddc.a-star.edu.sg thkeller@eddc.a-star.edu.sg rui.zhao@cuanschutz.edu cbkang@eddc.a-star.edu.sg.

Rui Zhao (R)

Department of Biochemistry and Molecular Genetics, University of Colorado Denver Anschutz Medical Campus, Aurora, Colorado. heide.ford@cuanschutz.edu jhill@eddc.a-star.edu.sg thkeller@eddc.a-star.edu.sg rui.zhao@cuanschutz.edu cbkang@eddc.a-star.edu.sg.

Heide L Ford (HL)

Department of Pharmacology, University of Colorado Denver Anschutz Medical Campus, Aurora, Colorado. heide.ford@cuanschutz.edu jhill@eddc.a-star.edu.sg thkeller@eddc.a-star.edu.sg rui.zhao@cuanschutz.edu cbkang@eddc.a-star.edu.sg.
Department of Biochemistry and Molecular Genetics, University of Colorado Denver Anschutz Medical Campus, Aurora, Colorado.

CongBao Kang (C)

Experimental Drug Discovery Centre, A*STAR, Singapore, Singapore. heide.ford@cuanschutz.edu jhill@eddc.a-star.edu.sg thkeller@eddc.a-star.edu.sg rui.zhao@cuanschutz.edu cbkang@eddc.a-star.edu.sg.

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Classifications MeSH