Composition determination for quaternary III-V semiconductors by aberration-corrected STEM.

Composition determination Image simulation Quantitative STEM Quaternary III-V semiconductors

Journal

Ultramicroscopy
ISSN: 1879-2723
Titre abrégé: Ultramicroscopy
Pays: Netherlands
ID NLM: 7513702

Informations de publication

Date de publication:
Nov 2019
Historique:
received: 25 04 2019
revised: 04 07 2019
accepted: 07 07 2019
pubmed: 17 7 2019
medline: 17 7 2019
entrez: 17 7 2019
Statut: ppublish

Résumé

Quantitative scanning transmission electron microscopy (STEM) is a powerful tool for the characterization of nano-materials. Absolute composition determination for ternary III-V semiconductors by direct comparison of experiment and simulation is well established. Here, we show a method to determine the composition of quaternary III-V semiconductors with two elements on each sub lattice from the intensities of one STEM image. As an example, this is applied to (GaIn)(AsBi). The feasibility of the method is shown in a simulation study that also explores the influence of detector angles and specimen thickness. Additionally, the method is applied to an experimental STEM image of a (GaIn)(AsBi) quantum well grown by metal organic vapour phase epitaxy. The obtained concentrations are in good agreement with X-ray diffraction and photoluminescence results.

Identifiants

pubmed: 31310886
pii: S0304-3991(19)30121-4
doi: 10.1016/j.ultramic.2019.112814
pii:
doi:

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

112814

Informations de copyright

Copyright © 2019 Elsevier B.V. All rights reserved.

Auteurs

P Kükelhan (P)

Materials Science Centre and Faculty of Physics, Philipps University Marburg, Hans-Meerwein-Straße 6, Marburg, Germany.

T Hepp (T)

Materials Science Centre and Faculty of Physics, Philipps University Marburg, Hans-Meerwein-Straße 6, Marburg, Germany.

S Firoozabadi (S)

Materials Science Centre and Faculty of Physics, Philipps University Marburg, Hans-Meerwein-Straße 6, Marburg, Germany.

A Beyer (A)

Materials Science Centre and Faculty of Physics, Philipps University Marburg, Hans-Meerwein-Straße 6, Marburg, Germany. Electronic address: andreas.beyer@physik.uni-marburg.de.

K Volz (K)

Materials Science Centre and Faculty of Physics, Philipps University Marburg, Hans-Meerwein-Straße 6, Marburg, Germany.

Classifications MeSH