Effect of pressure variation on the efficiency of supercritical fluid extraction of wild carrot (Daucus carota subsp. maritimus) extracts.


Journal

Journal of chromatography. B, Analytical technologies in the biomedical and life sciences
ISSN: 1873-376X
Titre abrégé: J Chromatogr B Analyt Technol Biomed Life Sci
Pays: Netherlands
ID NLM: 101139554

Informations de publication

Date de publication:
01 Sep 2019
Historique:
received: 07 05 2019
revised: 26 06 2019
accepted: 08 07 2019
pubmed: 20 7 2019
medline: 18 12 2019
entrez: 20 7 2019
Statut: ppublish

Résumé

The present study was conducted to check the comparative qualities of essential oils prepared by hydrodistillation (HD) and supercritical fluid techniques. It constitutes the first attempt to investigate the chemical composition of Daucus carota subsp. maritimus extracts using supercritical fluid technology (SFE) as an environmentally clean innovative method of extraction. The effect of pressure on the nature of extractable substances from wild carrot has been performed at a constant temperature of 50 °C and two different pressures (100 and 300 bar). The experimental results showed that pressure had a significant enhancing effect on the fluid transport properties and therefore on yield values. The extraction yield increases from 1.167 to 2.986% while increasing pressure. The chemical compositions of the essential oils prepared by HD and SFE were analyzed on the basis of gas chromatography-mass spectroscopy (GC-MS). Thus, we noticed that all analyzed samples were enriched in geranyl acetate and β‑bisabolene, and that the quantities of different identified substances were extremely sensitive to the extraction method and to the pressure variation in case of SFE.

Identifiants

pubmed: 31323559
pii: S1570-0232(19)30714-7
doi: 10.1016/j.jchromb.2019.121713
pii:
doi:

Substances chimiques

Acetates 0
Acyclic Monoterpenes 0
Monocyclic Sesquiterpenes 0
Oils, Volatile 0
Plant Oils 0
geranyl acetate 3W81YG7P9R
beta-bisabolene S19BRC22QA

Types de publication

Evaluation Study Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

121713

Informations de copyright

Copyright © 2019 Elsevier B.V. All rights reserved.

Auteurs

Siwar Majdoub (S)

Research Unit 13ES63, Applied Chemistry and Environment, Monastir University, Faculty of Sciences of Monastir, Monastir 5000, University of Monastir, Tunisia.

Ridha El Mokni (R)

Department of Life Sciences, Laboratory of Botany and Plant Ecology, Faculty of Sciences of Bizerta, Jarzouna-7021, Bizerta, University of Carthage, Tunisia; Department Pharmaceutical Sciences "A", Laboratory of Botany, Cryptogamy and Plant Biology, Faculty of Pharmacy of Monastir, BP 207, Avenue Avicenna-5000, University of Monastir, Tunisia; Department of Silvo-Pastoral Resources, Laboratory of Silvo-Pastoral Resources, Silvo-Pastoral Institute of Tabarka, BP. 345, Tabarka 8110, University of Jendouba, Tunisia.

Aliev Aslan Muradalievich (AA)

Mountain Botanical Garden DSC RAS, Yaragskogo Street, 75, Makhachkala 367030, Russia; Institute of Physics DSC RAS, Yaragskogo Street, 94, Makhachkala 367003, Russia.

Alessandra Piras (A)

Department of Chemical and Geological Science, University of Cagliari, Cittadella Universitaria di Monserrato, S.P. Monserrato-Sestu km 0,700, 09042 Monserrato, Italy.

Silvia Porcedda (S)

Department of Chemical and Geological Science, University of Cagliari, Cittadella Universitaria di Monserrato, S.P. Monserrato-Sestu km 0,700, 09042 Monserrato, Italy.

Saoussen Hammami (S)

Research Unit 13ES63, Applied Chemistry and Environment, Monastir University, Faculty of Sciences of Monastir, Monastir 5000, University of Monastir, Tunisia. Electronic address: h_saoussen@yahoo.fr.

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