Effect of pressure variation on the efficiency of supercritical fluid extraction of wild carrot (Daucus carota subsp. maritimus) extracts.
Daucus carota subsp. maritimus
Geranyl acetate
Hydrodistillation
Supercritical carbon dioxide extraction
Journal
Journal of chromatography. B, Analytical technologies in the biomedical and life sciences
ISSN: 1873-376X
Titre abrégé: J Chromatogr B Analyt Technol Biomed Life Sci
Pays: Netherlands
ID NLM: 101139554
Informations de publication
Date de publication:
01 Sep 2019
01 Sep 2019
Historique:
received:
07
05
2019
revised:
26
06
2019
accepted:
08
07
2019
pubmed:
20
7
2019
medline:
18
12
2019
entrez:
20
7
2019
Statut:
ppublish
Résumé
The present study was conducted to check the comparative qualities of essential oils prepared by hydrodistillation (HD) and supercritical fluid techniques. It constitutes the first attempt to investigate the chemical composition of Daucus carota subsp. maritimus extracts using supercritical fluid technology (SFE) as an environmentally clean innovative method of extraction. The effect of pressure on the nature of extractable substances from wild carrot has been performed at a constant temperature of 50 °C and two different pressures (100 and 300 bar). The experimental results showed that pressure had a significant enhancing effect on the fluid transport properties and therefore on yield values. The extraction yield increases from 1.167 to 2.986% while increasing pressure. The chemical compositions of the essential oils prepared by HD and SFE were analyzed on the basis of gas chromatography-mass spectroscopy (GC-MS). Thus, we noticed that all analyzed samples were enriched in geranyl acetate and β‑bisabolene, and that the quantities of different identified substances were extremely sensitive to the extraction method and to the pressure variation in case of SFE.
Identifiants
pubmed: 31323559
pii: S1570-0232(19)30714-7
doi: 10.1016/j.jchromb.2019.121713
pii:
doi:
Substances chimiques
Acetates
0
Acyclic Monoterpenes
0
Monocyclic Sesquiterpenes
0
Oils, Volatile
0
Plant Oils
0
geranyl acetate
3W81YG7P9R
beta-bisabolene
S19BRC22QA
Types de publication
Evaluation Study
Journal Article
Langues
eng
Sous-ensembles de citation
IM
Pagination
121713Informations de copyright
Copyright © 2019 Elsevier B.V. All rights reserved.