Development and validation of a dried blood spot test for thiamine deficiency among infants by HPLC-fluorimetry.
HPLC-fluorimetry
dried blood spot
infants
thiamine deficiency
thiamine diphosphate
Journal
Biomedical chromatography : BMC
ISSN: 1099-0801
Titre abrégé: Biomed Chromatogr
Pays: England
ID NLM: 8610241
Informations de publication
Date de publication:
Nov 2019
Nov 2019
Historique:
received:
29
09
2018
revised:
20
07
2019
accepted:
24
07
2019
pubmed:
30
7
2019
medline:
16
1
2020
entrez:
30
7
2019
Statut:
ppublish
Résumé
Thiamine deficiency, if detected early in infancy, can be treated with thiamine supplementation and can prevent seizures, other disabilities and death. The dried blood spot (DBS) sampling technique is an attractive sample collection technique for infants. The present study reports the development and validation of a highly sensitive and precise method for quantification of thiamine diphosphate from DBS. The method utilizes full-spot analysis of a volumetrically deposited 40 μl DBS. The analyte was extracted from the DBS using 50% methanol and then derivatized using potassium ferricyanide to thiochrome. Separation was achieved with the help of an Inertsil ODS C
Substances chimiques
Thiamine
X66NSO3N35
Types de publication
Journal Article
Langues
eng
Sous-ensembles de citation
IM
Pagination
e4668Subventions
Organisme : Vision Group of Science and Technology
ID : GRD-308
Organisme : Grand Challenges Canada
ID : R-ST-POC-1707-07275
Informations de copyright
© 2019 John Wiley & Sons, Ltd.
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