Quantifying Microsecond Exchange in Large Protein Complexes with Accelerated Relaxation Dispersion Experiments in the Solid State.
Journal
Scientific reports
ISSN: 2045-2322
Titre abrégé: Sci Rep
Pays: England
ID NLM: 101563288
Informations de publication
Date de publication:
31 07 2019
31 07 2019
Historique:
received:
15
01
2019
accepted:
16
07
2019
entrez:
2
8
2019
pubmed:
2
8
2019
medline:
21
10
2020
Statut:
epublish
Résumé
Solid state NMR is a powerful method to obtain information on the structure and dynamics of protein complexes that, due to solubility and size limitations, cannot be achieved by other methods. Here, we present an approach that allows the quantification of microsecond conformational exchange in large protein complexes by using a paramagnetic agent to accelerate
Identifiants
pubmed: 31366983
doi: 10.1038/s41598-019-47507-8
pii: 10.1038/s41598-019-47507-8
pmc: PMC6668460
doi:
Substances chimiques
Immunoglobulin G
0
Proteins
0
Types de publication
Journal Article
Research Support, N.I.H., Extramural
Research Support, Non-U.S. Gov't
Langues
eng
Sous-ensembles de citation
IM
Pagination
11082Subventions
Organisme : NIGMS NIH HHS
ID : P41 GM103311
Pays : United States
Organisme : Biotechnology and Biological Sciences Research Council
ID : BB/L022761/1
Pays : United Kingdom
Organisme : NIGMS NIH HHS
ID : R01 GM129325
Pays : United States
Organisme : Biotechnology and Biological Sciences Research Council
ID : BB/R010218/1
Pays : United Kingdom
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