Mass spectrometry imaging as a tool for evaluating the pulmonary distribution of exogenous surfactant in premature lambs.


Journal

Respiratory research
ISSN: 1465-993X
Titre abrégé: Respir Res
Pays: England
ID NLM: 101090633

Informations de publication

Date de publication:
05 Aug 2019
Historique:
received: 07 05 2019
accepted: 24 07 2019
entrez: 7 8 2019
pubmed: 7 8 2019
medline: 29 1 2020
Statut: epublish

Résumé

The amount of surfactant deposited in the lungs and its overall pulmonary distribution determine the therapeutic outcome of surfactant replacement therapy. Most of the currently available methods to determine the intrapulmonary distribution of surfactant are time-consuming and require surfactant labelling. Our aim was to assess the potential of Mass Spectrometry Imaging (MSI) as a label-free technique to qualitatively and quantitatively evaluate the distribution of surfactant to the premature lamb. Twelve preterm lambs (gestational age 126-127d, term ~150d) were allocated in two experimental groups. Seven lambs were treated with an intratracheal bolus of the synthetic surfactant CHF5633 (200 mg/kg) and 5 lambs were managed with mechanical ventilation for 120 min, as controls. The right lung lobes of all lambs were gradually frozen while inflated to 20 cmH Surfactant treatment was associated with a significant improvement of the mean arterial oxygenation and lung compliance (p < 0.05). Nevertheless, the physiological response to surfactant treatment was not uniform across all animals. SP-C analog and SP-B analog were successfully imaged and quantified by means of MSI in the peripheral lungs of all surfactant-treated animals. The intensity of the signal was remarkably low in untreated lambs, corresponding to background noise. The signal intensity of SP-B analog in each surfactant-treated animal, which represents the surfactant distributed to the peripheral right lung, correlated well with the physiologic response as assessed by the area under the curves of the individual arterial partial oxygen pressure and dynamic lung compliance curves of the lambs. Applying MSI, we were able to detect, locate and quantify the amount of exogenous surfactant distributed to the lower right lung of surfactant-treated lambs. The distribution pattern of SP-B analog correlated well with the pulmonary physiological outcomes of the animals. MSI is a valuable label-free technique which is able to simultaneously evaluate qualitative and quantitative drug distribution in the lung.

Sections du résumé

BACKGROUND BACKGROUND
The amount of surfactant deposited in the lungs and its overall pulmonary distribution determine the therapeutic outcome of surfactant replacement therapy. Most of the currently available methods to determine the intrapulmonary distribution of surfactant are time-consuming and require surfactant labelling. Our aim was to assess the potential of Mass Spectrometry Imaging (MSI) as a label-free technique to qualitatively and quantitatively evaluate the distribution of surfactant to the premature lamb.
METHODS METHODS
Twelve preterm lambs (gestational age 126-127d, term ~150d) were allocated in two experimental groups. Seven lambs were treated with an intratracheal bolus of the synthetic surfactant CHF5633 (200 mg/kg) and 5 lambs were managed with mechanical ventilation for 120 min, as controls. The right lung lobes of all lambs were gradually frozen while inflated to 20 cmH
RESULTS RESULTS
Surfactant treatment was associated with a significant improvement of the mean arterial oxygenation and lung compliance (p < 0.05). Nevertheless, the physiological response to surfactant treatment was not uniform across all animals. SP-C analog and SP-B analog were successfully imaged and quantified by means of MSI in the peripheral lungs of all surfactant-treated animals. The intensity of the signal was remarkably low in untreated lambs, corresponding to background noise. The signal intensity of SP-B analog in each surfactant-treated animal, which represents the surfactant distributed to the peripheral right lung, correlated well with the physiologic response as assessed by the area under the curves of the individual arterial partial oxygen pressure and dynamic lung compliance curves of the lambs.
CONCLUSIONS CONCLUSIONS
Applying MSI, we were able to detect, locate and quantify the amount of exogenous surfactant distributed to the lower right lung of surfactant-treated lambs. The distribution pattern of SP-B analog correlated well with the pulmonary physiological outcomes of the animals. MSI is a valuable label-free technique which is able to simultaneously evaluate qualitative and quantitative drug distribution in the lung.

Identifiants

pubmed: 31382955
doi: 10.1186/s12931-019-1144-5
pii: 10.1186/s12931-019-1144-5
pmc: PMC6683365
doi:

Substances chimiques

CHF5633 0
Peptide Fragments 0
Phosphatidylcholines 0
Pulmonary Surfactant-Associated Protein B 0
Pulmonary Surfactant-Associated Protein C 0
Pulmonary Surfactants 0

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

175

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Auteurs

Riccardo Zecchi (R)

Mass Spectrometry Service Center (CISM), University of Florence, Florence, Italy.

Pietro Franceschi (P)

Computational Biology, Research and Innovation Centre, Fondazione Edmund Mach, S. Michele all'Adige, TN, Italy.

Laura Tigli (L)

Preclinical R&D, Chiesi Farmaceutici, Largo Francesco Belloli, 11/A, 43122, Parma, Italy.

Francesca Ricci (F)

Preclinical R&D, Chiesi Farmaceutici, Largo Francesco Belloli, 11/A, 43122, Parma, Italy.

Francesca Boscaro (F)

Mass Spectrometry Service Center (CISM), University of Florence, Florence, Italy.

Barbara Pioselli (B)

Preclinical R&D, Chiesi Farmaceutici, Largo Francesco Belloli, 11/A, 43122, Parma, Italy.

Valentina Mileo (V)

Preclinical R&D, Chiesi Farmaceutici, Largo Francesco Belloli, 11/A, 43122, Parma, Italy.

Xabier Murgia (X)

Scientific Consultancy, Saarbrücken, Germany.

Federico Bianco (F)

Preclinical R&D, Chiesi Farmaceutici, Largo Francesco Belloli, 11/A, 43122, Parma, Italy.

Fabrizio Salomone (F)

Preclinical R&D, Chiesi Farmaceutici, Largo Francesco Belloli, 11/A, 43122, Parma, Italy. f.salomone@chiesi.com.

Augusto F Schmidt (AF)

Division of Neonatology and Pulmonary Biology, Cincinnati Children's Hospital, Cincinnati, USA.

Noah H Hillman (NH)

Division of Neonatology, Cardinal Glennon Children's Hospital, Saint Louis University, Saint Louis, USA.

Matthew W Kemp (MW)

Division of Obstetrics and Gynecology, University of Western Australia, Perth, WA, Australia.

Alan H Jobe (AH)

Division of Neonatology, Cardinal Glennon Children's Hospital, Saint Louis University, Saint Louis, USA.
Division of Obstetrics and Gynecology, University of Western Australia, Perth, WA, Australia.

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Classifications MeSH