Supercritical fluid extraction in isolation of cyclitols and sugars from chamomile flowers.
chamomile
cyclitols isolation
response surface methodology
sugars isolation
supercritical fluid extraction
Journal
Journal of separation science
ISSN: 1615-9314
Titre abrégé: J Sep Sci
Pays: Germany
ID NLM: 101088554
Informations de publication
Date de publication:
Oct 2019
Oct 2019
Historique:
revised:
22
07
2019
received:
31
05
2019
accepted:
11
08
2019
pubmed:
25
8
2019
medline:
25
8
2019
entrez:
25
8
2019
Statut:
ppublish
Résumé
The aim of the present study was to develop an optimization procedure for supercritical fluid extraction parameters, in order to obtain the highest possible yield of sugars and cyclitols from plant material. Response surface methodology based on Box-Behnken design was applied to evaluate the effect of: temperature (40, 60, 80°C), pressure (100, 200, 300 bar), and co-solvent (methanol) percentage (20, 25, 30%). As a result of the optimization process, we found that the highest amount of sugars (15.02 mg/gof dried material) and cyclitols (0.86 mg/g of dried material) was obtained when the following parameters were applied: 80°C, 228 bar, and 30% of methanol. Moreover, co-solvent concentration and temperature had a higher influence onto the obtained amounts compared with the pressure.
Identifiants
pubmed: 31444853
doi: 10.1002/jssc.201900539
doi:
Types de publication
Journal Article
Langues
eng
Sous-ensembles de citation
IM
Pagination
3243-3252Informations de copyright
© 2019 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.
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