Multi-residue ultra-performance liquid chromatography coupled with tandem mass spectrometry method for comprehensive multi-class anthropogenic compounds of emerging concern analysis in a catchment-based exposure-driven study.

Analysis Chemicals of emerging concern Environment Mass spectrometry

Journal

Analytical and bioanalytical chemistry
ISSN: 1618-2650
Titre abrégé: Anal Bioanal Chem
Pays: Germany
ID NLM: 101134327

Informations de publication

Date de publication:
Nov 2019
Historique:
received: 21 06 2019
accepted: 13 08 2019
revised: 26 07 2019
pubmed: 9 9 2019
medline: 9 9 2019
entrez: 9 9 2019
Statut: ppublish

Résumé

This paper presents a new multi-residue method for the quantification of more than 142 anthropogenic compounds of emerging concern (CECs) in various environmental matrices. These CECs are from a wide range of major classes including pharmaceuticals, household, industrial and agricultural. This method utilises ultra-performance liquid chromatography coupled with tandem mass spectrometry (UPLC-MS/MS) for analysis of five matrices (three liquid and two solid) from wastewater treatment processes and the surrounding environment. Relative recoveries were predominantly between 80 and 120%; however, due to the complexity of the matrices used in this work, not all compounds were recovered in all matrices, from 138/142 analytes in surface water to 96/142 analytes in digested solids. Method quantification limits (MQLs) ranged from 0.004 ng L

Identifiants

pubmed: 31494686
doi: 10.1007/s00216-019-02091-8
pii: 10.1007/s00216-019-02091-8
pmc: PMC6838033
doi:

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

7061-7086

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Auteurs

Kathryn Proctor (K)

Department of Chemistry, University of Bath, Claverton Down, Bath, BA2 7AY, UK.
Water Innovation & Research Centre, Department of Chemical Engineering, University of Bath, Claverton Down, Bath, BA2 7AY, UK.

Bruce Petrie (B)

Department of Chemistry, University of Bath, Claverton Down, Bath, BA2 7AY, UK.
School of Pharmacy and Life Sciences, Robert Gordon University, Aberdeen, AB10 7JG, UK.

Ruth Barden (R)

Wessex Water Services Ltd., Claverton Down, Bath, BA2 7WW, UK.

Tom Arnot (T)

Water Innovation & Research Centre, Department of Chemical Engineering, University of Bath, Claverton Down, Bath, BA2 7AY, UK.

Barbara Kasprzyk-Hordern (B)

Department of Chemistry, University of Bath, Claverton Down, Bath, BA2 7AY, UK. B.Kasprzyk-Hordern@bath.ac.uk.
Water Innovation & Research Centre, Department of Chemical Engineering, University of Bath, Claverton Down, Bath, BA2 7AY, UK. B.Kasprzyk-Hordern@bath.ac.uk.

Classifications MeSH