Snapshots of Dynamic Adaptation: Two-Dimensional Molecular Architectonics with Linear Bis-Hydroxamic Acid Modules.

atomic force microscopy host-guest systems hydroxamic acid scanning tunneling microscopy two-dimensional nanostructures

Journal

Angewandte Chemie (International ed. in English)
ISSN: 1521-3773
Titre abrégé: Angew Chem Int Ed Engl
Pays: Germany
ID NLM: 0370543

Informations de publication

Date de publication:
19 Dec 2019
Historique:
received: 25 09 2019
pubmed: 2 11 2019
medline: 2 11 2019
entrez: 1 11 2019
Statut: ppublish

Résumé

Linear modules equipped with two terminal hydroxamic acid groups act as the building block of diverse two-dimensional supramolecular motifs and patterns with room-temperature stability on the close-packed single-crystal surfaces of silver and gold, revealing a complex self-assembly scenario. By combining multiple investigation techniques (scanning tunneling microscopy, atomic force microscopy, X-ray photoelectron spectroscopy, and density functional theory calculations), we analyze the characteristics of the ordered assemblies which range from close-packed structures to polyporous networks featuring an exceptionally extended primitive unit cell with a side length exceeding 7 nm. The polyporous network shows potential for hosting and promoting the formation of chiral supramolecules, whereas a transition from 1D chiral randomness to an ordered racemate is discovered in a different porous phase. We correlate the observed structural changes to the adaptivity of the building block and surface-induced changes in the chemical state of the hydroxamic acid functional group.

Identifiants

pubmed: 31671244
doi: 10.1002/anie.201912247
pmc: PMC6973039
doi:

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

18948-18956

Subventions

Organisme : Horizon 2020
ID : 664878
Organisme : H2020 European Research Council
ID : 615233
Organisme : Deutsche Forschungsgemeinschaft
ID : 267156538
Organisme : Deutsche Forschungsgemeinschaft
ID : EXC 158
Organisme : Postdoctoral Research Foundation of China
Organisme : China Scholarship Council
Organisme : Max Planck Research School of Advanced Photon Science

Informations de copyright

© 2019 The Authors. Published by Wiley-VCH Verlag GmbH & Co. KGaA.

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Auteurs

Chao Jing (C)

Physics Department E20, Technical University of Munich, James Franck Straße 1, 85748, Garching, Germany.
Key Laboratory for Advanced Materials, School of Chemistry and Molecular Engineering, East China University of Science and Technology, Shanghai, 200237, P. R. China.

Bodong Zhang (B)

Physics Department E20, Technical University of Munich, James Franck Straße 1, 85748, Garching, Germany.

Sabine Synkule (S)

Physics Department E20, Technical University of Munich, James Franck Straße 1, 85748, Garching, Germany.

Maryam Ebrahimi (M)

Physics Department E20, Technical University of Munich, James Franck Straße 1, 85748, Garching, Germany.
Department of Chemistry, Lakehead University, 955 Oliver Rd, Thunder Bay, ON, P7B 5E1, Canada.

Alexander Riss (A)

Physics Department E20, Technical University of Munich, James Franck Straße 1, 85748, Garching, Germany.

Willi Auwärter (W)

Physics Department E20, Technical University of Munich, James Franck Straße 1, 85748, Garching, Germany.

Li Jiang (L)

Physics Department E20, Technical University of Munich, James Franck Straße 1, 85748, Garching, Germany.

Guillaume Médard (G)

Chair of Proteomics and Bioanalytics, Technical University of Munich, Emil Erlenmeyer Forum 5, 85354, Freising, Germany.

Joachim Reichert (J)

Physics Department E20, Technical University of Munich, James Franck Straße 1, 85748, Garching, Germany.

Johannes V Barth (JV)

Physics Department E20, Technical University of Munich, James Franck Straße 1, 85748, Garching, Germany.

Anthoula C Papageorgiou (AC)

Physics Department E20, Technical University of Munich, James Franck Straße 1, 85748, Garching, Germany.

Classifications MeSH