Salt Mediated Self-Assembly of Poly(ethylene glycol)-Functionalized Gold Nanorods.


Journal

Scientific reports
ISSN: 2045-2322
Titre abrégé: Sci Rep
Pays: England
ID NLM: 101563288

Informations de publication

Date de publication:
30 Dec 2019
Historique:
received: 10 10 2019
accepted: 16 12 2019
entrez: 1 1 2020
pubmed: 1 1 2020
medline: 1 1 2020
Statut: epublish

Résumé

Although challenging, assembling and orienting non-spherical nanomaterials into two- and three-dimensional (2D and 3D) ordered arrays can facilitate versatile collective properties by virtue of their shape-dependent properties that cannot be realized with their spherical counterparts. Here, we report on the self-assembly of gold nanorods (AuNRs) into 2D films at the vapor/liquid interface facilitated by grafting them with poly(ethylene glycol) (PEG). Using surface sensitive synchrotron grazing incidence small angle X-ray scattering (GISAXS) and specular X-ray reflectivity (XRR), we show that PEG-AuNRs in aqueous suspensions migrate to the vapor/liquid interface in the presence of salt, forming a uniform monolayer with planar-to-surface orientation. Furthermore, the 2D assembled PEG functionalized AuNRs exhibit short range order into rectangular symmetry with side-by-side and tail-to-tail nearest-neighbor packing. The effect of PEG chain length and salt concentration on the 2D assembly are also reported.

Identifiants

pubmed: 31889079
doi: 10.1038/s41598-019-56730-2
pii: 10.1038/s41598-019-56730-2
pmc: PMC6937238
doi:

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

20349

Subventions

Organisme : Basic Energy Sciences
ID : DE-AC02-07CH11358
Organisme : Basic Energy Sciences
ID : DE-AC02-07CH11358
Organisme : Basic Energy Sciences
ID : DE-AC02-07CH11358
Organisme : Basic Energy Sciences
ID : DE-AC02-07CH11358
Organisme : Basic Energy Sciences
ID : DE-AC02-07CH11358
Organisme : Basic Energy Sciences
ID : DE-AC02-07CH11358
Organisme : Basic Energy Sciences
ID : DE-AC02-07CH11358
Organisme : Basic Energy Sciences
ID : DE-AC02-07CH11358
Organisme : National Science Foundation
ID : NSF/CHE-1834750

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Auteurs

Hyeong Jin Kim (HJ)

Ames Laboratory, and Department of Chemical and Biological Engineering, Iowa State University, Ames, Iowa, 50011, United States.

Wenjie Wang (W)

Division of Materials Sciences and Engineering, Ames Laboratory, Iowa State University, Ames, Iowa, 50011, United States.

Wei Bu (W)

NSF's ChemMatCARS, University of Chicago, Illinois, 60637, United States.

Md Mir Hossen (MM)

Ames Laboratory, and Department of Chemical and Biological Engineering, Iowa State University, Ames, Iowa, 50011, United States.

Alejandra Londoño-Calderon (A)

Division of Materials Sciences and Engineering, Ames Laboratory, Iowa State University, Ames, Iowa, 50011, United States.

Andrew C Hillier (AC)

Ames Laboratory, and Department of Chemical and Biological Engineering, Iowa State University, Ames, Iowa, 50011, United States.

Tanya Prozorov (T)

Division of Materials Sciences and Engineering, Ames Laboratory, Iowa State University, Ames, Iowa, 50011, United States.

Surya Mallapragada (S)

Ames Laboratory, and Department of Chemical and Biological Engineering, Iowa State University, Ames, Iowa, 50011, United States. suryakm@iastate.edu.

David Vaknin (D)

Ames Laboratory, and Department of Physics and Astronomy, Iowa State University, Ames, Iowa, 50011, United States. vaknin@ameslab.gov.

Classifications MeSH