I-Optimal Design of Hierarchical 3D Scaffolds Produced by Combining Additive Manufacturing and Thermally Induced Phase Separation.

3D plotting additive manufacturing bone tissue engineering design of experiments (DoE) macro/microporous scaffolds thermally induced phase separation

Journal

ACS applied bio materials
ISSN: 2576-6422
Titre abrégé: ACS Appl Bio Mater
Pays: United States
ID NLM: 101729147

Informations de publication

Date de publication:
18 Feb 2019
Historique:
entrez: 17 1 2020
pubmed: 17 1 2020
medline: 17 1 2020
Statut: ppublish

Résumé

The limitations in the transport of oxygen, nutrients, and metabolic waste products pose a challenge to the development of bioengineered bone of clinically relevant size. This paper reports the design and characterization of hierarchical macro/microporous scaffolds made of poly(lactic-co-glycolic) acid and nanohydroxyapatite (PLGA/nHA). These scaffolds were produced by combining additive manufacturing (AM) and thermally induced phase separation (TIPS) techniques. Macrochannels with diameters of ~300 μm, ~380 μm, and ~460 μm were generated by embedding porous 3D-plotted polyethylene glycol (PEG) inside PLGA/nHA/1,4-dioxane or PLGA/1,4-dioxane solutions, followed by PEG extraction using deionized (DI) water. We have used an I-optimal design of experiments (DoE) and the response surface analysis (JMP® software) to relate three responses (scaffold thickness, porosity, and modulus) to the four experimental factors affecting the scaffold macro/microstructures (

Identifiants

pubmed: 31942566
doi: 10.1021/acsabm.8b00534
pmc: PMC6961819
mid: NIHMS1064124
doi:

Types de publication

Journal Article

Langues

eng

Pagination

685-696

Subventions

Organisme : NIAMS NIH HHS
ID : R15 AR066269
Pays : United States

Déclaration de conflit d'intérêts

Conflict of Interest Disclosure The authors declare no competing financial interest.

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Auteurs

Azizeh-Mitra Yousefi (AM)

Department of Chemical, Paper and Biomedical Engineering, Miami University, Oxford, OH 45056.

Junyi Liu (J)

Department of Chemical, Paper and Biomedical Engineering, Miami University, Oxford, OH 45056.

Riley Sheppard (R)

Department of Chemical, Paper and Biomedical Engineering, Miami University, Oxford, OH 45056.

Songmi Koo (S)

Department of Chemical, Paper and Biomedical Engineering, Miami University, Oxford, OH 45056.

Joshua Silverstein (J)

Department of Geology, Miami University, Oxford, OH 45056.

Jing Zhang (J)

Department of Statistics, Miami University, Oxford, OH 45056.

Paul F James (PF)

Department of Biology, Miami University, Oxford, OH 45056.

Classifications MeSH