Synthesis and Biological Evaluation of Heterocyclic Substituted Bis(indolyl)methanes.


Journal

Current organic synthesis
ISSN: 1570-1794
Titre abrégé: Curr Org Synth
Pays: United Arab Emirates
ID NLM: 101208457

Informations de publication

Date de publication:
2020
Historique:
received: 04 11 2019
revised: 14 12 2019
accepted: 09 01 2020
pubmed: 25 1 2020
medline: 18 5 2021
entrez: 25 1 2020
Statut: ppublish

Résumé

Bis(indolyl)methane derivatives are widely found in nature with a broad range of biological and pharmacological activities. The development of techniques for the synthesis and functionalization of bis(indolyl)methanes have attracted more and more attention in recent years. To study the synthesis and biological activity of heterocyclic substituted bis(indolyl)methanes. A series of heterocyclic substituted bis(indolyl)methanes (3a-3p) have been prepared by condensation reaction of indole and heterocyclic aldehydes catalyzed by boron trifluoride etherate with high yields. Preliminary in vitro anti-inflammatory in lipopolysaccharide (LPS)-stimulated RAW-264.7 macrophages and cytotoxic activity against human tumor cell lines (A549, Hela and SGC7901) by MTT assay were tested. The result indicated that heterocyclic substituted bis(indolyl)methanes showed good antiinflammatory and selective cytotoxic activity. Especially, compounds 3o, 3p and 3q displayed similar inhibitory effect on the generation of NO to positive control dexamethasone, and compound 3q displayed similar selective cytotoxic activity to 5-FU. Heterocyclic substituted bis(indolyl)methanes may be used as potential anti-inflammatory and anticancer leads.

Sections du résumé

BACKGROUND
Bis(indolyl)methane derivatives are widely found in nature with a broad range of biological and pharmacological activities. The development of techniques for the synthesis and functionalization of bis(indolyl)methanes have attracted more and more attention in recent years.
OBJECTIVE
To study the synthesis and biological activity of heterocyclic substituted bis(indolyl)methanes.
MATERIALS AND METHODS
A series of heterocyclic substituted bis(indolyl)methanes (3a-3p) have been prepared by condensation reaction of indole and heterocyclic aldehydes catalyzed by boron trifluoride etherate with high yields. Preliminary in vitro anti-inflammatory in lipopolysaccharide (LPS)-stimulated RAW-264.7 macrophages and cytotoxic activity against human tumor cell lines (A549, Hela and SGC7901) by MTT assay were tested.
RESULTS
The result indicated that heterocyclic substituted bis(indolyl)methanes showed good antiinflammatory and selective cytotoxic activity. Especially, compounds 3o, 3p and 3q displayed similar inhibitory effect on the generation of NO to positive control dexamethasone, and compound 3q displayed similar selective cytotoxic activity to 5-FU.
CONCLUSION
Heterocyclic substituted bis(indolyl)methanes may be used as potential anti-inflammatory and anticancer leads.

Identifiants

pubmed: 31976840
pii: COS-EPUB-103890
doi: 10.2174/1570179417666200124103400
doi:

Substances chimiques

Anti-Inflammatory Agents 0
Antineoplastic Agents 0
Indoles 0
Nitric Oxide 31C4KY9ESH

Types de publication

Journal Article Research Support, Non-U.S. Gov't

Langues

eng

Sous-ensembles de citation

IM

Pagination

144-150

Informations de copyright

Copyright© Bentham Science Publishers; For any queries, please email at epub@benthamscience.net.

Auteurs

Min-Xin Li (MX)

College of Pharmaceutical Science, Yunnan University of Chinese Medicine, Kunming 650500, China.

Xiao-Jia Pu (XJ)

College of Pharmaceutical Science, Yunnan University of Chinese Medicine, Kunming 650500, China.

Xia Zhang (X)

College of Pharmaceutical Science, Yunnan University of Chinese Medicine, Kunming 650500, China.

Xi Zheng (X)

Central Laboratory, The NO.1 Affiliated Hospital of Yunnan University of Chinese Medicine, Kunming 650021, China.

Hui Gao (H)

College of Pharmaceutical Science, Yunnan University of Chinese Medicine, Kunming 650500, China.

Wei-Lie Xiao (WL)

Key Laboratory of Medicinal Chemistry for Natural Resource, Ministry of Education and Yunnan Province, School of Chemical Science and Technology, Yunnan University, Kunming 650091, China.

Chun-Ping Wan (CP)

Central Laboratory, The NO.1 Affiliated Hospital of Yunnan University of Chinese Medicine, Kunming 650021, China.

Ze-Wei Mao (ZW)

College of Pharmaceutical Science, Yunnan University of Chinese Medicine, Kunming 650500, China.

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Classifications MeSH