Determination of phenytoin in exhaled breath condensate using electromembrane extraction followed by capillary electrophoresis.
Capillary electrophoresis
Central composite design
Electromembrane extraction
Exhaled breath condensate
Phenytoin
Journal
Electrophoresis
ISSN: 1522-2683
Titre abrégé: Electrophoresis
Pays: Germany
ID NLM: 8204476
Informations de publication
Date de publication:
05 2020
05 2020
Historique:
received:
09
10
2019
revised:
09
01
2020
accepted:
21
01
2020
pubmed:
6
2
2020
medline:
1
4
2021
entrez:
6
2
2020
Statut:
ppublish
Résumé
Application of hollow fiber-based electromembrane extraction was studied for extraction and quantification of phenytoin from exhaled breath condensate (EBC). Phenytoin is extracted from EBC through a supported liquid membrane consisting of 1-octanol impregnated in the walls of a hollow fiber, and into an alkaline aqueous acceptor solution inside the lumen of the fiber. Under the obtained conditions of electromembrane extraction, that is, the extraction time of 15 min, stirring speed of 750 rpm, donor phase pH at 11.0, acceptor pH at 13.0, and an applied voltage of 15 V across the supported liquid membrane, an enrichment factor of 102-fold correspond to extraction percent of 25.5% was achieved. Good linearity was obtained over the concentration range of 0.001-0.10 µg/mL (r
Identifiants
pubmed: 32022289
doi: 10.1002/elps.201900440
doi:
Substances chimiques
Anticonvulsants
0
Membranes, Artificial
0
Phenytoin
6158TKW0C5
Types de publication
Journal Article
Research Support, Non-U.S. Gov't
Langues
eng
Sous-ensembles de citation
IM
Pagination
666-677Subventions
Organisme : Pharmaceutical Analysis Research Center, Tabriz University of Medical Sciences
ID : 61555
Pays : International
Informations de copyright
© 2020 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.
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