Combined X-ray and neutron single-crystal diffraction in diamond anvil cells.
diamond anvil cells
high pressure
single-crystal X-ray diffraction
single-crystal neutron diffraction
Journal
Journal of applied crystallography
ISSN: 0021-8898
Titre abrégé: J Appl Crystallogr
Pays: United States
ID NLM: 9876190
Informations de publication
Date de publication:
01 Feb 2020
01 Feb 2020
Historique:
received:
12
08
2019
accepted:
17
10
2019
entrez:
13
2
2020
pubmed:
13
2
2020
medline:
13
2
2020
Statut:
epublish
Résumé
It is shown that it is possible to perform combined X-ray and neutron single-crystal studies in the same diamond anvil cell (DAC). A modified Merrill-Bassett DAC equipped with an inflatable membrane filled with He gas has been developed. It can be used on laboratory X-ray and synchrotron diffractometers as well as on neutron instruments. The data processing procedures and a joint structural refinement of the high-pressure synchrotron and neutron single-crystal data are presented and discussed for the first time.
Identifiants
pubmed: 32047402
doi: 10.1107/S1600576719014201
pii: pd5113
pmc: PMC6998780
doi:
Types de publication
Journal Article
Langues
eng
Pagination
9-14Informations de copyright
© Andrzej Grzechnik et al. 2020.
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