EANM guideline on the validation of analytical methods for radiopharmaceuticals.

Radioanalytical methods Radiopharmaceuticals Validation

Journal

EJNMMI radiopharmacy and chemistry
ISSN: 2365-421X
Titre abrégé: EJNMMI Radiopharm Chem
Pays: England
ID NLM: 101714628

Informations de publication

Date de publication:
12 Feb 2020
Historique:
received: 11 09 2019
accepted: 19 12 2019
entrez: 14 2 2020
pubmed: 14 2 2020
medline: 14 2 2020
Statut: epublish

Résumé

To fulfil good manufacturing requirements, analytical methods for the analysis of pharmaceuticals for human and vetinary use must be validated. The International Conference on Harmonization of Technical Requirements for Registration of Pharmaceuticals for Human Use (ICH) has published guidance documents on the requirements for such validation activities and these have been adopted by the European Medicines Agency, The U.S. Food and Drug Administration (FDA) and other regulatory bodies. These guidance documents do not, however, fully address all the specific tests required for the analysis of radiopharmaceuticals. This guideline attempts to rectify this shortcoming, by recommending approaches to validate such methods. Recommedations for the validation of analytical methods which are specific for radiopharmaceutials are presented in this guideline, along with two practical examples. In order to comply with good manufacturing practice, analytical methods for radiopharmaceuticals for human use should be validated.

Sections du résumé

BACKGROUND BACKGROUND
To fulfil good manufacturing requirements, analytical methods for the analysis of pharmaceuticals for human and vetinary use must be validated. The International Conference on Harmonization of Technical Requirements for Registration of Pharmaceuticals for Human Use (ICH) has published guidance documents on the requirements for such validation activities and these have been adopted by the European Medicines Agency, The U.S. Food and Drug Administration (FDA) and other regulatory bodies. These guidance documents do not, however, fully address all the specific tests required for the analysis of radiopharmaceuticals. This guideline attempts to rectify this shortcoming, by recommending approaches to validate such methods.
RESULTS RESULTS
Recommedations for the validation of analytical methods which are specific for radiopharmaceutials are presented in this guideline, along with two practical examples.
CONCLUSIONS CONCLUSIONS
In order to comply with good manufacturing practice, analytical methods for radiopharmaceuticals for human use should be validated.

Identifiants

pubmed: 32052212
doi: 10.1186/s41181-019-0086-z
pii: 10.1186/s41181-019-0086-z
pmc: PMC7016057
doi:

Types de publication

Journal Article

Langues

eng

Pagination

7

Références

Pharmaceuticals (Basel). 2014 May 14;7(5):621-33
pubmed: 24830987
J Pharm Biomed Anal. 2015;111:209-14
pubmed: 25898315
Nucl Med Biol. 1993 Apr;20(3):367-9
pubmed: 8485498

Auteurs

Nic Gillings (N)

Department of Clinical Physiology, Nuclear Medicine and PET, Copenhagen University Hospital Rigshospitalet, Blegdamsvej 9, DK-2100, Copenhagen, Denmark. ngil0001@regionh.dk.

Sergio Todde (S)

Tecnomed Foundation, University of Milano - Bicocca, Milan, Italy.

Martin Behe (M)

Center for Radiopharmaceutical Sciences, Paul Scherrer Institute, Villigen, Switzerland.

Clemens Decristoforo (C)

Department of Nuclear Medicine, Medical University Innsbruck, Innsbruck, Austria.

Philip Elsinga (P)

Department of Nuclear Medicine and Molecular Imaging, University Medical Center Groningen, Groningen, The Netherlands.

Valentina Ferrari (V)

MSD Animal Health, Walton, UK.

Olaug Hjelstuen (O)

Institute for Energy Technology (IFE), Kjeller, Norway.

Petra Kolenc Peitl (PK)

University Medical Centre Ljubljana, Ljubljana, Slovenia.

Jacek Koziorowski (J)

Independant consultant, Linköbing, Sweden.

Peter Laverman (P)

Radboud University Medical Center Nijmegen, Nijmegen, The Netherlands.

Thomas L Mindt (TL)

Ludwig Boltzmann Institute Applied Diagnostics, Vienna, Austria.

Meltem Ocak (M)

Department of Pharmaceutical Technology, Istanbul University, Istanbul, Turkey.

Marianne Patt (M)

Department for Nuclear Medicine, University Hospital Leipzig, Leipzig, Germany.

Classifications MeSH