A Ninhydrin-Type Urea Sorbent for the Development of a Wearable Artificial Kidney.


Journal

Macromolecular bioscience
ISSN: 1616-5195
Titre abrégé: Macromol Biosci
Pays: Germany
ID NLM: 101135941

Informations de publication

Date de publication:
03 2020
Historique:
received: 18 11 2019
revised: 09 01 2020
pubmed: 18 2 2020
medline: 6 1 2021
entrez: 18 2 2020
Statut: ppublish

Résumé

The aim of this study is to develop polymeric chemisorbents with a high density of ninhydrin groups, able to covalently bind urea under physiological conditions and thus potentially suitable for use in a wearable artificial kidney. Macroporous beads are prepared by suspension polymerization of 5-vinyl-1-indanone (vinylindanone) using a 90:10 (v/v) mixture of toluene and nitrobenzene as a porogen. The indanone groups are subsequently oxidized in a one-step procedure into ninhydrin groups. Their urea absorption kinetics are evaluated under both static and dynamic conditions at 37 °C in simulated dialysate (urea in phosphate buffered saline). Under static conditions and at a 1:1 molar ratio of ninhydrin: urea the sorbent beads remove ≈0.6-0.7 mmol g

Identifiants

pubmed: 32065727
doi: 10.1002/mabi.201900396
doi:

Substances chimiques

Urea 8W8T17847W
Ninhydrin HCL6S9K23A

Types de publication

Journal Article Research Support, Non-U.S. Gov't

Langues

eng

Sous-ensembles de citation

IM

Pagination

e1900396

Informations de copyright

© 2020 The Authors. Published by WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

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Auteurs

Jacobus A W Jong (JAW)

Department of Pharmaceutics, Utrecht Institute for Pharmaceutical Sciences (UIPS), Utrecht University, Universiteitsweg 99, 3584 CG, Utrecht, the Netherlands.
Department of Nephrology and Hypertension, University Medical Centre Utrecht, 3584 CX, Utrecht, the Netherlands.

Yong Guo (Y)

Department of Pharmaceutics, Utrecht Institute for Pharmaceutical Sciences (UIPS), Utrecht University, Universiteitsweg 99, 3584 CG, Utrecht, the Netherlands.

Diënty Hazenbrink (D)

Department of Nephrology and Hypertension, University Medical Centre Utrecht, 3584 CX, Utrecht, the Netherlands.

Stefania Douka (S)

Department of Pharmaceutics, Utrecht Institute for Pharmaceutical Sciences (UIPS), Utrecht University, Universiteitsweg 99, 3584 CG, Utrecht, the Netherlands.

Dennis Verdijk (D)

MercaChem B.V., Kerkenbos 1013, 6546 BB, Nijmegen, the Netherlands.

Johan van der Zwan (J)

NMR Spectroscopy, Bijvoet Center for Biomolecular Research, Utrecht University, Padualaan 8, 3584 CH, Utrecht, the Netherlands.

Klaartje Houben (K)

NMR Spectroscopy, Bijvoet Center for Biomolecular Research, Utrecht University, Padualaan 8, 3584 CH, Utrecht, the Netherlands.

Marc Baldus (M)

NMR Spectroscopy, Bijvoet Center for Biomolecular Research, Utrecht University, Padualaan 8, 3584 CH, Utrecht, the Netherlands.

Karina C Scheiner (KC)

Department of Pharmaceutics, Utrecht Institute for Pharmaceutical Sciences (UIPS), Utrecht University, Universiteitsweg 99, 3584 CG, Utrecht, the Netherlands.

Remco Dalebout (R)

Inorganic Chemistry and Catalysis, Debye Institute for Nanomaterials Science, Utrecht University, Universiteitsweg 99, 3584 CG, Utrecht, the Netherlands.

Marianne C Verhaar (MC)

Department of Nephrology and Hypertension, University Medical Centre Utrecht, 3584 CX, Utrecht, the Netherlands.

Robert Smakman (R)

Innovista, Raadhuisstraat 1, 1393 NW, Nigtevecht, the Netherlands.

Wim E Hennink (WE)

Department of Pharmaceutics, Utrecht Institute for Pharmaceutical Sciences (UIPS), Utrecht University, Universiteitsweg 99, 3584 CG, Utrecht, the Netherlands.

Karin G F Gerritsen (KGF)

Department of Nephrology and Hypertension, University Medical Centre Utrecht, 3584 CX, Utrecht, the Netherlands.

Cornelus F van Nostrum (CF)

Department of Pharmaceutics, Utrecht Institute for Pharmaceutical Sciences (UIPS), Utrecht University, Universiteitsweg 99, 3584 CG, Utrecht, the Netherlands.

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