The HXD95: a modified Bassett-type hydrothermal diamond-anvil cell for in situ XRD experiments up to 5 GPa and 1300 K.
diamond-anvil cells
extreme conditions
glasses and melts
metallic liquids
resistive heating
synchrotron characterization
Journal
Journal of synchrotron radiation
ISSN: 1600-5775
Titre abrégé: J Synchrotron Radiat
Pays: United States
ID NLM: 9888878
Informations de publication
Date de publication:
01 Mar 2020
01 Mar 2020
Historique:
received:
22
07
2019
accepted:
16
12
2019
entrez:
11
3
2020
pubmed:
11
3
2020
medline:
11
3
2020
Statut:
ppublish
Résumé
A new diamond-anvil cell apparatus for in situ synchrotron X-ray diffraction measurements of liquids and glasses, at pressures from ambient to 5 GPa and temperatures from ambient to 1300 K, is reported. This portable setup enables in situ monitoring of the melting of complex compounds and the determination of the structure and properties of melts under moderately high pressure and high temperature conditions relevant to industrial processes and magmatic processes in the Earth's crust and shallow mantle. The device was constructed according to a modified Bassett-type hydrothermal diamond-anvil cell design with a large angular opening (θ = 95°). This paper reports the successful application of this device to record in situ synchrotron X-ray diffraction of liquid Ga and synthetic PbSiO
Identifiants
pubmed: 32153294
pii: S1600577519016801
doi: 10.1107/S1600577519016801
pmc: PMC7064104
doi:
Types de publication
Journal Article
Langues
eng
Sous-ensembles de citation
IM
Pagination
529-537Subventions
Organisme : Natural Environment Research Council
ID : NE/M000117/1
Organisme : Natural Environment Research Council
ID : NE/M00046X/1
Organisme : Natural Environment Research Council
ID : NE/M000419/1
Informations de copyright
open access.
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