Fabrication of Nanoyttria by Method of Solution Combustion Synthesis.
DIL
DTA
DTG
FT-IR
SCS
yttria nanopowder
Journal
Nanomaterials (Basel, Switzerland)
ISSN: 2079-4991
Titre abrégé: Nanomaterials (Basel)
Pays: Switzerland
ID NLM: 101610216
Informations de publication
Date de publication:
27 Apr 2020
27 Apr 2020
Historique:
received:
06
04
2020
revised:
24
04
2020
accepted:
24
04
2020
entrez:
1
5
2020
pubmed:
1
5
2020
medline:
1
5
2020
Statut:
epublish
Résumé
In the work the research on properties of an yttria nanopowder obtained by solution combustion synthesis (SCS) in terms of its application in ceramic technology is presented. In order to characterize the SCS reaction the decomposition of yttrium nitrate, glycine and their solution was investigated using differential thermal analysis coupled with FT-IR spectrometry of the gases emitted during the measurements. The product obtained in the SCS process was characterized in terms of its microstructure, particle size distribution and BET specific surface. Although the obtained powders showed nanoscaled structures, only after calcination at a temperature of 1100 °C nanosized particles were revealed. The calcined powder occurred in an agglomerated state (cumulants mean Z
Identifiants
pubmed: 32349286
pii: nano10050831
doi: 10.3390/nano10050831
pmc: PMC7712192
pii:
doi:
Types de publication
Journal Article
Langues
eng
Subventions
Organisme : Ministerstwo Nauki i Szkolnictwa Wyższego
ID : Praca została sfinansowana ze środków na działalność statutową Instytutu Ceramiki i Materiałów Budowlanych.
Déclaration de conflit d'intérêts
The authors declare no conflict of interest.
Références
Phys Chem Chem Phys. 2015 Jan 14;17(2):1325-31
pubmed: 25424414
Materials (Basel). 2014 Sep 19;7(9):6768-6778
pubmed: 28788211
Adv Mater. 2015 Dec 16;27(47):7874-80
pubmed: 26484846
Chem Rev. 2016 Dec 14;116(23):14493-14586
pubmed: 27610827
Annu Rev Chem Biomol Eng. 2012;3:103-27
pubmed: 22468598
Nanomaterials (Basel). 2019 Aug 22;9(9):
pubmed: 31443571