Development and validation of a spectrofluorimetric method for the analysis of tolfenamic acid in pure and tablet dosage form.
spectrofluorimetric assay
stability
tolfenamic acid
validation
Journal
Luminescence : the journal of biological and chemical luminescence
ISSN: 1522-7243
Titre abrégé: Luminescence
Pays: England
ID NLM: 100889025
Informations de publication
Date de publication:
Nov 2020
Nov 2020
Historique:
received:
23
11
2019
revised:
16
02
2020
accepted:
01
04
2020
pubmed:
19
5
2020
medline:
1
7
2021
entrez:
19
5
2020
Statut:
ppublish
Résumé
Tolfenamic acid (TA) is commonly used in humans and animals because of its anti-inflammatory, antipyretic, and analgesic effects. So far, no study has been carried out to develop a validated spectrofluorimetric method for determination of TA. Therefore, the present study aimed to develop and validate a simple, accurate, rapid, economical, and precise spectrofluorimetric method to assay TA in its pure and dosage forms, and also in degraded solutions. The fluorimetric method had higher sensitivity compared with the spectrophotometric and high-performance liquid chromatography methods and could determine the drug at the microgram level. Optimum pH of TA for maximum fluorescence intensity was 3, and its two pK
Substances chimiques
Tablets
0
ortho-Aminobenzoates
0
tolfenamic acid
3G943U18KM
Types de publication
Journal Article
Langues
eng
Sous-ensembles de citation
IM
Pagination
1017-1027Subventions
Organisme : Higher Education Commission, Pakistan
ID : 5263
Informations de copyright
© 2020 John Wiley & Sons, Ltd.
Références
S. Sweetman (Ed), Martindale The Complete Drug Reference, Pharmaceutical Press, London, UK 2013 1689.
British National Formulary (BNF) 76, BMJ Group and Royal Pharmaceutical Society, Pharmaceutical Press, London, UK 2018 469.
P. J. Pentikainen, P. J. Neuvonen, C. Backman, Eur. J. Clin. Pharmacol. 1981, 19, 359.
S. Ahmed, M. A. Sheraz, I. U. Rehman, AAPS PharmSciTech 2013, 14, 870.
S. Ahmed, M. A. Sheraz, I. Ahmad, Profiles of Drug Substances, Excipients, and Related Methodology, Vol. 43, Academic Press, Elsevier, Cambridge, USA 2018 255.
R. Basha, S. F. Connelly, U. T. Sankpal, G. P. Nagaraju, H. Patel, J. K. Vishwanatha, S. Shelake, L. Tabor-Simecka, M. Shoji, J. W. Simecka, B. El-Rayes, J. Nutr. Biochem. 2016, 31, 77.
T. Jittreetat, Y. S. Shin, H. S. Hwang, B. S. Lee, Y. S. Kim, P. Sannikorn, C. H. Kim, Yonsei Med. J. 2016, 57, 588.
F. U. Ertem, W. Zhang, K. Chang, W. Mohaiza Dashwood, P. Rajendran, D. Sun, A. Abudayyeh, E. Vilar, M. Abdelrahim, R. H. Dashwood, Int. J. Cancer 2017, 140, 460.
R. Parveen, B. Sravanthi, P. Dastidar, Chem. - Asian J. 2017, 12, 792.
S. Shelake, U. T. Sankpal, W. Paul Bowman, M. Wise, A. Ray, R. Basha, Invest. New Drugs 2017, 35, 158.
H. Kruszewska, T. Zareba, S. Tyski, Acta Pol. Pharm. 2002, 59, 436.
P. C. Andrews, R. L. Ferrero, P. C. Junk, I. Kumar, Q. Luu, K. Nguyen, J. W. Taylor, Dalton Trans. 2010, 39, 2861.
W. J. Wilson, M. F. Afzali, J. E. Cummings, M. E. Legare, R. B. Tjalkens, C. P. Allen, R. A. Slayden, W. H. Hanneman, PLoS Negl. Trop. Dis. 2016, 10, e0005065.
L. Pan, C. L. Gardner, F. A. Pagliai, C. F. Gonzalez, G. L. Lorca, Front. Microbiol. 2017, 8, 1591.
L. I. Adwan, R. Basha, M. Abdelrahim, G. M. Subaiea, N. H. Zawia, Curr. Alzheimer Res. 2011, 8, 385.
L. Adwan, G. M. Subaiea, N. H. Zawia, Neuropharmacology 2014, 79, 596.
L. Adwan, G. M. Subaiea, R. Basha, N. H. Zawia, J. Neurochem. 2015, 133, 266.
G. M. Subaiea, B. Alansi, D. Serra, M. Alwan, N. Zawia, Curr. Alzheimer Res. 2011, 8, 860.
G. M. Subaiea, L. I. Adwan, A. H. Ahmed, K. E. Stevens, N. H. Zawia, Neurobiol. Aging 2013, 34, 2421.
G. M. Subaiea, A. H. Ahmed, L. I. Adwan, N. H. Zawia, J. Alzheimers Dis. 2015, 43, 425.
P. C. Ioannou, N. V. Rusakova, D. A. Andrikopoulou, K. M. Glynou, G. M. Tzompanaki, Analyst 1998, 123, 2839.
M. Zampakou, N. Rizeq, V. Tangoulis, A. N. Papadopoulos, F. Perdih, I. Turel, G. Psomas, Inorg. Chem. 2014, 53, 2040.
British Pharmacopoeia, Her Majesty's Stationary Office, London, UK, 2019 Electronic version.
N. S. Abdelwahab, N. W. Ali, M. M. Zaki, M. Abdelkawy, J. Chromatogr. Sci. 2015, 53, 484.
K. V. Andersen, S. Larsen, B. Alhede, N. Gelting, O. Buchardt, J. Chem. Soc. Perkin Trans. 1989, 2, 1443.
A. Mattei, T. Li, Pharm. Res. 2012, 29, 460.
M. A. Sheraz, S. Ahmed, I. U. Rehman, Pharm. Dev. Technol. 2015, 20, 352.
A. O. Surov, I. V. Terekhova, A. Bauer-Brandl, G. L. Perlovich, Cryst. Growth Des. 2009, 9, 3265.
A. O. Surov, P. Szterner, W. Zielenkiewicz, G. L. Perlovich, J. Pharm. Biomed. Anal. 2009, 50, 831.
International Council for Harmonization, Validation of Analytical Procedures: Text and Methodology Q2 (R1), in International Council for Harmonization of Technical Requirements for Registration of Pharmaceuticals for Human Use, n/a, Geneva, Switzerland 2005.
S. Ahmed, M. A. Sheraz, C. Yorucu, I. U. Rehman, Cent. Eur. J. Chem. 2013, 11, 1533.
R. K. Gilpin, W. Zhou, J. Pharm. Biomed. Anal. 2005, 37, 509.
S. Jabeen, T. J. Dines, S. A. Leharne, B. Z. Chowdhry, Spectrochim. Acta A Mol. Biomol. Spectrosc. 2012, 96, 972.
P. Thybo, J. Kristensen, L. Hovgaard, Pharm. Dev. Technol. 2007, 12, 43.
A. Mattei, T. Li, Int. J. Pharm. 2011, 418, 179.
J. Saurina, S. Hernandez-Cassou, R. Tauler, A. Izquierdo-Ridorsa, Anal. Chim. Acta 2000, 408, 135.
J. Reijenga, A. van Hoof, A. van Loon, B. Teunissen, Anal. Chem. Insights 2013, 8, 53.
S. Rozou, E. Antoniadou-Vyza, J. Pharm. Biomed. Anal. 1998, 18, 899.
S. Rozou, S. Michaleas, E. Antoniadou-Vyza, Pharm. Pharmacol. Commun. 1999, 5, 79.
C. A. S. Bergstrom, C. M. Wassvik, K. Johansson, I. Hubatsch, J. Med. Chem. 2007, 50, 5858.
M. Polasek, M. Pospisilova, M. Urbanek, J. Pharm. Biomed. Anal. 2000, 23, 135.
L. S. Rosenberg, S. G. Schulman, J. Simons, Talanta 1979, 26, 867.
I. Ahmad, T. Mirza, S. G. Musharraf, Z. Anwar, M. A. Sheraz, S. Ahmed, M. A. Ejaz, A. Khurshid, RSC Adv. 2019, 9, 26559.
S. G. Schulman, A. C. Capomacchia, J. Phys. Chem. 1975, 79, 1337.
P. J. Sinko (Ed), Martin Physical Pharmacy and Pharmaceutical Sciences, 6th ed., Lippincott Williams & Wilkins, Philadelphia, USA 2011 318.
S. Hansen, S. Pedersen-Bjergaard, K. Rasmussen, Introduction to Pharmaceutical Chemical Analysis, John Wiley & Sons Ltd., Chichester, West Sussex, UK 2012 89.