Synthesis of Chiral MOF-74 Frameworks by Post-Synthetic Modification by Using an Amino Acid.

chiral induction chirality defects metal-organic frameworks post-synthetic modifications vibrational circular dichroism

Journal

Chemistry (Weinheim an der Bergstrasse, Germany)
ISSN: 1521-3765
Titre abrégé: Chemistry
Pays: Germany
ID NLM: 9513783

Informations de publication

Date de publication:
02 Nov 2020
Historique:
received: 08 05 2020
revised: 25 05 2020
pubmed: 28 5 2020
medline: 28 5 2020
entrez: 28 5 2020
Statut: ppublish

Résumé

The synthesis of chiral metal-organic frameworks (MOFs) is highly relevant for asymmetric heterogenous catalysis, yet very challenging. Chiral MOFs with MOF-74 topology were synthesised by using post-synthetic modification with proline. Vibrational circular dichroism studies demonstrate that proline is the source of chirality. The solvents used in the synthesis play a key role in tuning the loading of proline and its interaction with the MOF-74 framework. In N,N'-dimethylformamide, proline coordinates monodentate to the Zn

Identifiants

pubmed: 32459371
doi: 10.1002/chem.202002293
pmc: PMC7702064
doi:

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

13957-13965

Subventions

Organisme : Nederlandse Organisatie voor Wetenschappelijk Onderzoek
ID : 718.015.004

Informations de copyright

© 2020 The Authors. Published by Wiley-VCH GmbH.

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Auteurs

Andreea Gheorghe (A)

Van 't Hoff Institute for Molecular Sciences, University of Amsterdam, Science Park 904, 1098, XH, Amsterdam, The Netherlands.

Benjamin Strudwick (B)

Van 't Hoff Institute for Molecular Sciences, University of Amsterdam, Science Park 904, 1098, XH, Amsterdam, The Netherlands.
Current address: Paul Scherrer Institute, ETH Zürich, Forschungsstrasse 111, 5232 Villigen PSI, Zürich, Switzerland.

Daniel M Dawson (DM)

EaStCHEM School of Chemistry and Centre of Magnetic Resonance, University of St Andrews, North Haugh, KY16 9ST, St. Andrews, UK.

Sharon E Ashbrook (SE)

EaStCHEM School of Chemistry and Centre of Magnetic Resonance, University of St Andrews, North Haugh, KY16 9ST, St. Andrews, UK.

Sander Woutersen (S)

Van 't Hoff Institute for Molecular Sciences, University of Amsterdam, Science Park 904, 1098, XH, Amsterdam, The Netherlands.

David Dubbeldam (D)

Van 't Hoff Institute for Molecular Sciences, University of Amsterdam, Science Park 904, 1098, XH, Amsterdam, The Netherlands.

Stefania Tanase (S)

Van 't Hoff Institute for Molecular Sciences, University of Amsterdam, Science Park 904, 1098, XH, Amsterdam, The Netherlands.

Classifications MeSH