Fluctuation suppression in microgels by polymer electrolytes.


Journal

Structural dynamics (Melville, N.Y.)
ISSN: 2329-7778
Titre abrégé: Struct Dyn
Pays: United States
ID NLM: 101660872

Informations de publication

Date de publication:
May 2020
Historique:
received: 24 03 2020
accepted: 18 05 2020
entrez: 23 6 2020
pubmed: 23 6 2020
medline: 23 6 2020
Statut: epublish

Résumé

Structural details of thermoresponsive, cationically poly(N-iso-propylacrylamide-co-methacrylamido propyl trimethyl ammonium chloride) microgels and the influence of the anionic electrolyte polystyrene sulfonate (PSS) on the internal structure and dynamics of the cationic microgels have been studied with a combination of small angle neutron scattering (SANS) and neutron spin echo (NSE) spectroscopy. While SANS can yield information on the overall size of the particles and on the typical correlation length inside the particles, studying the segmental polymer dynamics with NSE gives access to more internal details, which only appear due to their effect on the polymer motion. The segmental dynamics of the microgels studied in this paper is to a large extent suppressed by the PSS additive. Possible scenarios of the influence of the polyanions on the microgel structure and dynamics are discussed.

Identifiants

pubmed: 32566697
doi: 10.1063/4.0000014
pii: 4.0000014
pmc: PMC7297544
doi:

Types de publication

Journal Article

Langues

eng

Pagination

034302

Informations de copyright

© 2020 Author(s).

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Auteurs

S Pasini (S)

Forschungszentrum Jülich GmbH, JCNS at Heinz Maier-Leibnitz Zentrum, Lichtenbergstraße 1, 85747 Garching, Germany.

S Maccarrone (S)

Forschungszentrum Jülich GmbH, JCNS at Heinz Maier-Leibnitz Zentrum, Lichtenbergstraße 1, 85747 Garching, Germany.

N K Székely (NK)

Forschungszentrum Jülich GmbH, JCNS at Heinz Maier-Leibnitz Zentrum, Lichtenbergstraße 1, 85747 Garching, Germany.

L R Stingaciu (LR)

NScD, Oak Ridge National Laboratory, Oak Ridge, Tennessee 37831, USA.

A P H Gelissen (APH)

Institute of Physical Chemistry, RWTH Aachen University, 52056 Aachen, Germany.

W Richtering (W)

Institute of Physical Chemistry, RWTH Aachen University, 52056 Aachen and JARA-SOFT 52056 Aachen, Germany.

M Monkenbusch (M)

Jülich Centre for Neutron Science (JCNS) & Institute for Complex Systems (ICS), Forschungszentrum Jülich GmbH, 52428 Jülich, Germany.

O Holderer (O)

Forschungszentrum Jülich GmbH, JCNS at Heinz Maier-Leibnitz Zentrum, Lichtenbergstraße 1, 85747 Garching, Germany.

Classifications MeSH