Nonclassical Recrystallization.

analytical ultracentrifugation mesocrystals nanocrystals recrystallization size separation

Journal

Chemistry (Weinheim an der Bergstrasse, Germany)
ISSN: 1521-3765
Titre abrégé: Chemistry
Pays: Germany
ID NLM: 9513783

Informations de publication

Date de publication:
26 Nov 2020
Historique:
received: 14 06 2020
pubmed: 23 6 2020
medline: 23 6 2020
entrez: 23 6 2020
Statut: ppublish

Résumé

Applications in the fields of materials science and nanotechnology increasingly demand monodisperse nanoparticles in size and shape. Up to now, no general purification procedure exists to thoroughly narrow the size and shape distributions of nanoparticles. Here, we show by analytical ultracentrifugation (AUC) as an absolute and quantitative high-resolution method that multiple recrystallizations of nanocrystals to mesocrystals is a very efficient tool to generate nanocrystals with an excellent and so-far unsurpassed size-distribution (PDI

Identifiants

pubmed: 32569441
doi: 10.1002/chem.202002873
pmc: PMC7756702
doi:

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

15242-15248

Subventions

Organisme : Deutsche Forschungsgemeinschaft
ID : SFB1214
Organisme : Universität Konstanz
ID : Zukunftskolleg and "Konstanzia Transition"
Organisme : European Research Council (ERC) under the Horizon 2020
ID : 715620

Informations de copyright

© 2020 The Authors. Published by Wiley-VCH GmbH.

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Auteurs

Julian Brunner (J)

Physical Chemistry, University of Konstanz, Universitätsstraße 10, 78457, Konstanz, Germany.

Britta Maier (B)

Physical Chemistry, University of Konstanz, Universitätsstraße 10, 78457, Konstanz, Germany.

Rose Rosenberg (R)

Physical Chemistry, University of Konstanz, Universitätsstraße 10, 78457, Konstanz, Germany.

Sebastian Sturm (S)

Institute for Solid State Research, Leibniz Institute for Solid State and Materials Research Dresden, Helmholzstraße 20, 01069, Dresden, Germany.

Helmut Cölfen (H)

Physical Chemistry, University of Konstanz, Universitätsstraße 10, 78457, Konstanz, Germany.

Elena V Sturm (EV)

Physical Chemistry, University of Konstanz, Universitätsstraße 10, 78457, Konstanz, Germany.

Classifications MeSH