MASS SPECTROMETRY-BASED TECHNIQUES FOR DIRECT QUANTIFICATION OF HIGH IONIZATION ENERGY ELEMENTS IN SOLID MATERIALS-CHALLENGES AND PERSPECTIVES.
direct determination
electronegative elements
element analysis
isotopic analysis
mass spectrometry
nonmetals
solid samples
Journal
Mass spectrometry reviews
ISSN: 1098-2787
Titre abrégé: Mass Spectrom Rev
Pays: United States
ID NLM: 8219702
Informations de publication
Date de publication:
07 2021
07 2021
Historique:
revised:
18
06
2020
received:
20
04
2020
accepted:
18
06
2020
pubmed:
4
7
2020
medline:
4
7
2020
entrez:
4
7
2020
Statut:
ppublish
Résumé
The determination of nonmetals, first of all, the most electronegative ones-nitrogen, oxygen, fluorine, chlorine, and bromine, poses the highest challenge for element analysis. These elements are characterized by high reactivity, volatility, high ionization energy, and the absence of intensive spectral lines in the optical spectral range. Conventional techniques of their quantification include considerable "wet chemistry" stages so the application of these techniques for the solid sample is highly laborious and prone to uncontrollable uncertainties. Additionally, current development in material science and other areas requires the quantification of the elements at lower levels with good sensitivity. Owing to their robustness and flexibility, mass spectrometry techniques provide vast possibilities for the quantification, spatial and isotopic analysis, including the solutions for direct analysis of solids. The current review focuses on the application of major mass spectrometric techniques for the quantification of N, O, F, Cl, and Br in solid samples. The following techniques are mainly considered: thermal ionization mass spectrometry (TIMS), isotope-ratio MS (IRMS), secondary ion MS (SIMS), inductively coupled plasma MS (ICP-MS), and glow discharge MS (GDMS); as the most accessible and widely applied for the purpose. General ionization issues, advantages, limitations, and novel methodological solutions are discussed. © 2020 John Wiley & Sons Ltd.
Types de publication
Journal Article
Review
Research Support, Non-U.S. Gov't
Langues
eng
Sous-ensembles de citation
IM
Pagination
359-380Informations de copyright
© 2020 John Wiley & Sons Ltd.
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