Indirect Determination of Amikacin by Gold Nanoparticles as Redox Probe.

Amikacin antibutics electrochemical sensor gold nanoparticles human serum. voltammetry

Journal

Current drug delivery
ISSN: 1875-5704
Titre abrégé: Curr Drug Deliv
Pays: United Arab Emirates
ID NLM: 101208455

Informations de publication

Date de publication:
2021
Historique:
received: 12 02 2020
revised: 16 03 2020
accepted: 25 04 2020
pubmed: 20 7 2020
medline: 3 11 2021
entrez: 20 7 2020
Statut: ppublish

Résumé

Amikacin is an aminoglycoside antibiotic used for many gram-negative bacterial infections like infections in the urinary tract, infections in brain, lungs and abdomen. Electrochemical determination of amikacin is a challenge in electroanalysis because it shows no voltammetric peak at the surface of bare electrodes. In this approach, a very simple and easy method for indirect voltammetric determination of amikacin presented in real samples. Gold nanoparticles were electrodeposited at the surface of glassy carbon electrode in constant potential. The effect of several parameters such as time and potential of deposition, pH and scan rates on signal were studied. The cathodic peak current of Au Two dynamic linear ranges of 1.0 × 10 The method was successfully determined amikacin in pharmaceutical preparation and human serum. The effect of several interference in determination of amikacin was also studied.

Sections du résumé

BACKGROUND BACKGROUND
Amikacin is an aminoglycoside antibiotic used for many gram-negative bacterial infections like infections in the urinary tract, infections in brain, lungs and abdomen. Electrochemical determination of amikacin is a challenge in electroanalysis because it shows no voltammetric peak at the surface of bare electrodes.
OBJECTIVE OBJECTIVE
In this approach, a very simple and easy method for indirect voltammetric determination of amikacin presented in real samples. Gold nanoparticles were electrodeposited at the surface of glassy carbon electrode in constant potential.
METHODS METHODS
The effect of several parameters such as time and potential of deposition, pH and scan rates on signal were studied. The cathodic peak current of Au
RESULTS RESULTS
Two dynamic linear ranges of 1.0 × 10
CONCLUSION CONCLUSIONS
The method was successfully determined amikacin in pharmaceutical preparation and human serum. The effect of several interference in determination of amikacin was also studied.

Identifiants

pubmed: 32682378
pii: CDD-EPUB-108260
doi: 10.2174/1567201817666200719005919
doi:

Substances chimiques

Gold 7440-57-5
Amikacin 84319SGC3C

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

761-769

Informations de copyright

Copyright© Bentham Science Publishers; For any queries, please email at epub@benthamscience.net.

Auteurs

Mansureh Alizadeh (M)

Department of Chemistry, University of Mohaghegh Ardabili, Ardabil, Iran.

Mandana Amiri (M)

Department of Chemistry, University of Mohaghegh Ardabili, Ardabil, Iran.

Abolfazl Bezaatpour (A)

Department of Chemistry, University of Mohaghegh Ardabili, Ardabil, Iran.

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Classifications MeSH