HPLC enantio-separation and chiral recognition mechanism of quinolones on vancomycin CSP.

Chromatography, High Pressure Liquid / methods Limit of Detection Linear Models Quinolones / analysis Reproducibility of Results Stereoisomerism Vancomycin / chemistry
Chiral recognition mechanism Enantio-separation Quinolones Vancomycin

Journal

Journal of chromatography. B, Analytical technologies in the biomedical and life sciences
ISSN: 1873-376X
Titre abrégé: J Chromatogr B Analyt Technol Biomed Life Sci
Pays: Netherlands
ID NLM: 101139554

Informations de publication

Date de publication:
10 Nov 2020
Historique:
received: 08 07 2020
revised: 08 08 2020
accepted: 16 08 2020
pubmed: 2 9 2020
medline: 23 4 2021
entrez: 2 9 2020
Statut: ppublish

Résumé

A new HPLC method was developed for the enantio-separation and chiral recognition mechanism of quinolones (lomefloxacine, ofloxacine, primaquine and quinacrine) on Vancomycin CSP. The column used was Chirabiotic V column (150 × 4.6 mm, 5.0 μm) with two mobile phases i.e. (I) MeOH:ACN:H

Identifiants

DOI: 10.1016/j.jchromb.2020.122335 PMID: 32871377
pubmed: 32871377
pii: S1570-0232(20)30990-9
doi: 10.1016/j.jchromb.2020.122335
pii:
doi:

Substances chimiques

Quinolones 0
Vancomycin 6Q205EH1VU

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

122335

Informations de copyright

Copyright © 2020 Elsevier B.V. All rights reserved.

Déclaration de conflit d'intérêts

Declaration of Competing Interest The authors declare that they have no known competing financial interests or personal relationships that could have appeared to influence the work reported in this paper.

Auteurs

Zeid A ALOthman (ZA)

Department of Chemistry, College of Science, King Saud University, P. O. Box 2455, Riyadh 11451, Saudi Arabia. Electronic address: zaothman@ksu.edu.sa.

Abdullah G ALanazi (AG)

Department of Chemistry, College of Science, King Saud University, P. O. Box 2455, Riyadh 11451, Saudi Arabia.

Mohd Suhail (M)

Department of Chemistry, Jamia Millia Islamia, Jamia Nagar, New Delhi 110025, India.

Imran Ali (I)

Department of Chemistry, Jamia Millia Islamia, Jamia Nagar, New Delhi 110025, India; Department of Chemistry, College of Sciences, Taibah University, Al-Medina Al-Munawara 41477, Saudi Arabia. Electronic address: drimran.chiral@gmail.com.

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Classifications MeSH

questionsmedicales.fr › Techniques d'investigation › Techniques de chimie analytique › Chromatographie › Chromatographie en phase liquide › Chromatographie en phase liquide à haute performance › HPLC enantio-separation and chiral recognition...
questionsmedicales.fr › Environnement et santé publique › Santé publique › Méthodes épidémiologiques › Statistiques comme sujet › Sensibilité et spécificité › Limite de détection › HPLC enantio-separation and chiral recognition...
questionsmedicales.fr › Environnement et santé publique › Santé publique › Méthodes épidémiologiques › Statistiques comme sujet › Analyse de régression › Modèles linéaires › HPLC enantio-separation and chiral recognition...
questionsmedicales.fr › Composés hétérocycliques › Composés hétérocycliques à cycles fusionnés › Composés hétérobicycliques › Quinoléines › Quinolinone › HPLC enantio-separation and chiral recognition...
questionsmedicales.fr › Environnement et santé publique › Santé publique › Méthodes épidémiologiques › Méthodologie en recherche épidémiologique › Reproductibilité des résultats › HPLC enantio-separation and chiral recognition...
questionsmedicales.fr › Phénomènes chimiques › Phénomènes de chimie organique › Isomérie › Stéréoisomérie › HPLC enantio-separation and chiral recognition...
questionsmedicales.fr › Acides aminés, peptides et protéines › Peptides › Glycopeptides › Vancomycine › HPLC enantio-separation and chiral recognition...