Addressing H-Material Interaction in Fast Diffusion Materials-A Feasibility Study on a Complex Phase Steel.

advanced high-strength steels hydrogen embrittlement in-situ testing plasma charging scanning electron microscopy

Journal

Materials (Basel, Switzerland)
ISSN: 1996-1944
Titre abrégé: Materials (Basel)
Pays: Switzerland
ID NLM: 101555929

Informations de publication

Date de publication:
20 Oct 2020
Historique:
received: 26 08 2020
revised: 05 10 2020
accepted: 16 10 2020
entrez: 23 10 2020
pubmed: 24 10 2020
medline: 24 10 2020
Statut: epublish

Résumé

Hydrogen embrittlement (HE) is one of the main limitations in the use of advanced high-strength steels in the automotive industry. To have a better understanding of the interaction between hydrogen (H) and a complex phase steel, an in-situ method with plasma charging was applied in order to provide continuous H supply during mechanical testing in order to avoid H outgassing. For such fast-H diffusion materials, only direct observation during in-situ charging allows for addressing H effects on materials. Different plasma charging conditions were analysed, yet there was not a pronounced effect on the mechanical properties. The H concentration was calculated while using a simple analytical model as well as a simulation approach, resulting in consistent low H values, below the critical concentration to produce embrittlement. However, the dimple size decreased in the presence of H and, with increasing charging time, the crack propagation rate increased. The rate dependence of flow properties of the material was also investigated, proving that the material has no strain rate sensitivity, which confirmed that the crack propagation rate increased due to H effects. Even though the H concentration was low in the experiments that are presented here, different technological alternatives can be implemented in order to increase the maximum solute concentration.

Identifiants

pubmed: 33092297
pii: ma13204677
doi: 10.3390/ma13204677
pmc: PMC7589168
pii:
doi:

Types de publication

Journal Article

Langues

eng

Subventions

Organisme : Österreichische Forschungsförderungsgesellschaft
ID : 859480

Références

Microsc Microanal. 2006 Feb;12(1):85-91
pubmed: 17481344
Materials (Basel). 2018 Apr 28;11(5):
pubmed: 29710803
Rev Sci Instrum. 2020 Apr 1;91(4):043705
pubmed: 32357725

Auteurs

Agustina Massone (A)

Materials Center Leoben, Forschungs GmbH, Roseggerstrasse 12, 8700 Leoben, Austria.
Department Materials Science, Chair of Materials Physics, Montanuniversität Leoben, Jahnstrasse 12, 8700 Leoben, Austria.

Armin Manhard (A)

Max-Planck-Institut für Plasmaphysik, Boltzmannstr. 2, D-85748 Garching, Germany.

Andreas Drexler (A)

Institut für Werkstoffkunde, Fügetechnik und Umformtechnik, Technische Universität Graz, Rechbauerstrasse 12, 8010 Graz, Austria.

Christian Posch (C)

Materials Center Leoben, Forschungs GmbH, Roseggerstrasse 12, 8700 Leoben, Austria.

Werner Ecker (W)

Materials Center Leoben, Forschungs GmbH, Roseggerstrasse 12, 8700 Leoben, Austria.

Verena Maier-Kiener (V)

Department Materials Science, Chair of Physically Metallurgy and Metallic Materials, Montanuniversität Leoben, Roseggerstrasse 12/Max-Tendler-Strasse 9, 8700 Leoben, Austria.

Daniel Kiener (D)

Department Materials Science, Chair of Materials Physics, Montanuniversität Leoben, Jahnstrasse 12, 8700 Leoben, Austria.

Classifications MeSH