Assessment of Melatonin and Its Precursors Content by a HPLC-MS/MS Method from Different Romanian Wines.


Journal

ACS omega
ISSN: 2470-1343
Titre abrégé: ACS Omega
Pays: United States
ID NLM: 101691658

Informations de publication

Date de publication:
27 Oct 2020
Historique:
received: 20 07 2020
accepted: 02 10 2020
entrez: 2 11 2020
pubmed: 3 11 2020
medline: 3 11 2020
Statut: epublish

Résumé

Because melatonin has strong antioxidant activity and wine is an alcoholic beverage of economic relevance, in the present work, the impact of some variable parameters that may occur in the winemaking process on the concentrations of melatonin and its precursors in Romanian wines was studied. Therefore, a sensitive and selective high-performance liquid chromatography-tandem mass spectrometry (HPLC-MS/MS) method was developed for the simultaneous analysis of melatonin, serotonin, and l-tryptophan, and some method performance parameters including selectivity, detection limit, precision (by comparing with an alternative HPLC-FL method), accuracy, and robustness were validated. These determinations are significant and the final amounts of analytes are dependent on the microorganisms involved in the winemaking process, the grape variety, geographic regions of vineyards, and aging of wines. In the future, the method may be useful to increase the melatonin content and the antioxidant activity in wines by improved steps in the winemaking process, especially based on application of selected yeasts and improved fermentation conditions.

Identifiants

pubmed: 33134687
doi: 10.1021/acsomega.0c03463
pmc: PMC7594137
doi:

Types de publication

Journal Article

Langues

eng

Pagination

27254-27260

Informations de copyright

© 2020 American Chemical Society.

Déclaration de conflit d'intérêts

The authors declare no competing financial interest.

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Auteurs

Camelia Albu (C)

Centre of Bioanalysis, National Institute of Research and Development for Biological Sciences-Bucharest, 296 Splaiul Independentei, 060031 Bucharest, Romania.

Letitia Elena Radu (LE)

Carol Davila University of Medicine and Pharmacy, 8 Eroii Sanitari Bulevard, 050474 Bucharest, Romania.

Gabriel-Lucian Radu (GL)

Centre of Bioanalysis, National Institute of Research and Development for Biological Sciences-Bucharest, 296 Splaiul Independentei, 060031 Bucharest, Romania.

Classifications MeSH