Preparation of multiwall carbon nanotube/urea-formaldehyde nanocomposite as a new sorbent in solid-phase extraction and its combination with deep eutectic solvent-based dispersive liquid-liquid microextraction for extraction of antibiotic residues in honey.
Adsorption
Anti-Bacterial Agents
/ analysis
Butanols
/ chemistry
Formaldehyde
/ chemistry
Honey
/ analysis
Liquid Phase Microextraction
Nanotubes, Carbon
/ chemistry
Particle Size
Pesticide Residues
/ analysis
Quaternary Ammonium Compounds
/ chemistry
Solid Phase Extraction
Solvents
/ chemistry
Surface Properties
Urea
/ chemistry
antibiotics
deep eutectic solvent
dispersive liquid-liquid extraction
honey
ion mobility spectrometry
solid-phase extraction
Journal
Journal of separation science
ISSN: 1615-9314
Titre abrégé: J Sep Sci
Pays: Germany
ID NLM: 101088554
Informations de publication
Date de publication:
Jan 2021
Jan 2021
Historique:
received:
18
06
2020
revised:
07
09
2020
accepted:
11
10
2020
pubmed:
6
11
2020
medline:
5
10
2021
entrez:
5
11
2020
Statut:
ppublish
Résumé
A solid-phase extraction method combined with deep eutectic solvent-based dispersive liquid-liquid microextraction has been developed for the extraction of three antibiotics in honey samples prior to their determination by ion mobility spectrometry. In this method, first, a multiwall carbon nanotube/urea-formaldehyde nanocomposite was synthesized using co-precipitation polymerization method and then it was used as a sorbent for the analytes extraction from the samples. After that the adsorbed analytes were eluted from the sorbent using a water-miscible organic solvent. The collected elution solvent was mixed with tetrabutylammonium chloride:butanol deep eutectic solvent and the mixture was applied in the following microextraction method. The method provided low limits of detection and quantification in the ranges of 0.32-0.86 and 1.1-2.9 ng/g, respectively. The method had a proper repeatability expressed as relative standard deviation less than or equal to 9.1%. The validated method was successfully performed on different honey samples obtained from different producers.
Identifiants
pubmed: 33151627
doi: 10.1002/jssc.202000679
doi:
Substances chimiques
Anti-Bacterial Agents
0
Butanols
0
Nanotubes, Carbon
0
Pesticide Residues
0
Quaternary Ammonium Compounds
0
Solvents
0
Formaldehyde
1HG84L3525
Urea
8W8T17847W
tetrabutylammonium
CBU2X6BBJR
Types de publication
Journal Article
Langues
eng
Sous-ensembles de citation
IM
Pagination
576-584Informations de copyright
© 2020 Wiley-VCH GmbH.
Références
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