Chemically Fueled Volume Phase Transition of Polyacid Microgels.

dissipative self-assembly fuels microgels nonequilibrium processes polymers

Journal

Angewandte Chemie (International ed. in English)
ISSN: 1521-3773
Titre abrégé: Angew Chem Int Ed Engl
Pays: Germany
ID NLM: 0370543

Informations de publication

Date de publication:
22 03 2021
Historique:
revised: 10 12 2020
received: 28 10 2020
pubmed: 20 12 2020
medline: 20 12 2020
entrez: 19 12 2020
Statut: ppublish

Résumé

Microgels are soft colloids that show responsive behavior and are easy to functionalize for applications. They are considered key components for future smart colloidal material systems. However, so far microgel systems have almost exclusively been studied in classical responsive switching settings using external triggers, while internally organized, autonomous control mechanisms as found in supramolecular chemistry and DNA nanotechnology relying on fuel-driven out-of-equilibrium concepts have not been implemented into microgel systems. Here, we introduce chemically fueled transient volume phase transitions (VPTs) for poly(methacrylic acid) (PMAA) microgels, where the collapsed hydrophobic state can be programmed using the fuel concentration in a cyclic reaction network. We discuss details of the system behavior as a function of pH and fuel amount, unravel kinetically trapped regions and showcase transient encapsulation and time-programmed release as a first application.

Identifiants

pubmed: 33340387
doi: 10.1002/anie.202014417
pmc: PMC8048534
doi:

Types de publication

Journal Article Research Support, Non-U.S. Gov't

Langues

eng

Sous-ensembles de citation

IM

Pagination

7117-7125

Informations de copyright

© 2020 The Authors. Angewandte Chemie International Edition published by Wiley-VCH GmbH.

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Auteurs

Jonas Heckel (J)

Institute for Macromolecular Chemistry, University of Freiburg, Stefan-Meier-Str. 31, 79104, Freiburg, Germany.
Freiburg Materials Research Center (FMF), University of Freiburg, Stefan-Meier-Str. 21, 79104, Freiburg, Germany.
Freiburg Center for Interactive Materials and Bioinspired Technologies (FIT), University of Freiburg, Georges-Köhler-Allee 105, 79110, Freiburg, Germany.

Sebastian Loescher (S)

Institute for Macromolecular Chemistry, University of Freiburg, Stefan-Meier-Str. 31, 79104, Freiburg, Germany.
Freiburg Materials Research Center (FMF), University of Freiburg, Stefan-Meier-Str. 21, 79104, Freiburg, Germany.
Freiburg Center for Interactive Materials and Bioinspired Technologies (FIT), University of Freiburg, Georges-Köhler-Allee 105, 79110, Freiburg, Germany.

Robert T Mathers (RT)

Department of Chemistry, Pennsylvania State University, New Kensington, PA, 15068, USA.

Andreas Walther (A)

A3BMS Lab, Department of Chemistry, University of Mainz, Duesbergweg 10-14, 55128, Mainz, Germany.
Cluster of Excellence livMatS @ FIT-Freiburg Center for Interactive Materials and Bioinspired Technologies, University of Freiburg, Georges-Köhler-Allee 105, 79110, Freiburg, Germany.

Classifications MeSH