Efficient Separation of Acetylene and Carbon Dioxide in a Decorated Zeolite.

acetylene gas separation neutron diffraction neutron scattering zeolites

Journal

Angewandte Chemie (International ed. in English)
ISSN: 1521-3773
Titre abrégé: Angew Chem Int Ed Engl
Pays: Germany
ID NLM: 0370543

Informations de publication

Date de publication:
15 Mar 2021
Historique:
received: 02 11 2020
revised: 11 12 2020
pubmed: 29 12 2020
medline: 29 12 2020
entrez: 28 12 2020
Statut: ppublish

Résumé

The almost identical molecular sizes and volatilities of acetylene and carbon dioxide make their separation extremely challenging in industry. Reported here is the efficient separation of acetylene and carbon dioxide (v/v=2/1, which is relevant to that in the industrial cracking stream) in faujasite zeolites decorated with atomically-dispersed copper(II) sites under ambient conditions. In situ neutron powder diffraction and inelastic neutron scattering confirm that the confined copper(II) site displays chemoselective yet reversible binding to acetylene, whereas adsorbed carbon dioxide molecules are stabilized by weak host-guest supramolecular interactions with the framework oxygen centers, thus resulting in the efficient separation of these two gases under flow conditions. A designed adsorption-purging-desorption system based upon Cu@FAU is established for the recovery of high purity acetylene (98-99 %) from the mixture of acetylene and carbon dioxide, offering an unprecedented separation factor of 22.2 with an effective dynamic uptake of acetylene of 1.51 mmol g

Identifiants

pubmed: 33368904
doi: 10.1002/anie.202014680
doi:

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

6526-6532

Subventions

Organisme : National Natural Science Foundation of China
ID : 22025203
Organisme : Municipal Natural Science Foundation of Tianjin
ID : 18JCJQJC47400
Organisme : The Royal Society
ID : NAF\R1\180297

Informations de copyright

© 2020 Wiley-VCH GmbH.

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Auteurs

Shanshan Liu (S)

School of Materials Science and Engineering & National Institute for Advanced Materials, Nankai University, Tianjin, 300350, China.

Xue Han (X)

Department of Chemistry, The University of Manchester, Manchester, M13 9PL, UK.

Yuchao Chai (Y)

School of Materials Science and Engineering & National Institute for Advanced Materials, Nankai University, Tianjin, 300350, China.

Guangjun Wu (G)

School of Materials Science and Engineering & National Institute for Advanced Materials, Nankai University, Tianjin, 300350, China.

Weiyao Li (W)

Department of Chemistry, The University of Manchester, Manchester, M13 9PL, UK.

Jiangnan Li (J)

Department of Chemistry, The University of Manchester, Manchester, M13 9PL, UK.

Ivan da Silva (I)

ISIS Facility, STFC, Rutherford Appleton Laboratory, Chilton, Oxfordshire, OX11 0QX, UK.

Pascal Manuel (P)

ISIS Facility, STFC, Rutherford Appleton Laboratory, Chilton, Oxfordshire, OX11 0QX, UK.

Yongqiang Cheng (Y)

Neutron Scattering Division, Neutron Sciences Directorate, Oak Ridge National Laboratory, Oak Ridge, TN, 37831, USA.

Luke L Daemen (LL)

Neutron Scattering Division, Neutron Sciences Directorate, Oak Ridge National Laboratory, Oak Ridge, TN, 37831, USA.

Anibal J Ramirez-Cuesta (AJ)

Neutron Scattering Division, Neutron Sciences Directorate, Oak Ridge National Laboratory, Oak Ridge, TN, 37831, USA.

Wei Shi (W)

College of Chemistry, Nankai University, Tianjin, 300071, China.

Naijia Guan (N)

School of Materials Science and Engineering & National Institute for Advanced Materials, Nankai University, Tianjin, 300350, China.

Sihai Yang (S)

Department of Chemistry, The University of Manchester, Manchester, M13 9PL, UK.

Landong Li (L)

School of Materials Science and Engineering & National Institute for Advanced Materials, Nankai University, Tianjin, 300350, China.

Classifications MeSH