In-situ formation of Zn-Al layered double oxides on electrochemically anodized nanoporous aluminum film as sorbent for chlorophenols extraction from water and wastewater followed by determination using HPLC.
Zn-Al layered double oxides
chlorophenols
thin film microextraction
wastewater samples
Journal
Journal of separation science
ISSN: 1615-9314
Titre abrégé: J Sep Sci
Pays: Germany
ID NLM: 101088554
Informations de publication
Date de publication:
Mar 2021
Mar 2021
Historique:
revised:
31
12
2020
received:
13
09
2020
accepted:
01
01
2021
pubmed:
6
1
2021
medline:
6
1
2021
entrez:
5
1
2021
Statut:
ppublish
Résumé
Herein, we present a simple, cost-effective, and robust strategy for the in-situ preparation of Zn-Al layered double oxides-anodized aluminum thin film via a facile hydrothermal method, followed by calcination treatment of the Zn-Al layered double hydroxide in the air atmosphere. The in-situ prepared Zn-Al layered double oxide-anodized aluminum film was implemented as sorbent for thin film microextraction of four selected chlorophenols (4-chlorophenol, 2,4-dichlorophenol, 2,4,6-trichlorophenol, and pentachlorophenol), followed by high-performance liquid chromatography-ultraviolet detection. The different variables of the thin film microextraction were screened via Plackett-Burman design and then optimized through Box-Behnken design. Under the optimum condition, the method showed good linear ranges (0.2-200 μg/L) with the coefficient of determinations higher than 0.9938. The calculated limit of detections were between 0.07 and 0.56 μg/L. Relative standard deviations of the method for determination of the analytes at 5 μg/L concentration level (n = 3) were ranged from 3.5 to 3.9% (as interday). The enrichment factors were between 39 and 58. This extraction method was demonstrated to be fast, efficient, and convenient. To study the capability of the developed method for real sample analysis, tap, well, river, and two types of wastewater samples were satisfactorily analyzed.
Identifiants
pubmed: 33400826
doi: 10.1002/jssc.202000993
doi:
Types de publication
Journal Article
Langues
eng
Sous-ensembles de citation
IM
Pagination
1264-1272Subventions
Organisme : the Iran National Science Foundation (INSF)
ID : 98009196
Informations de copyright
© 2021 Wiley-VCH GmbH.
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