Functionalization of Chitosan Oligomers: From Aliphatic Epoxide to Cardanol-Grafted Oligomers for Oil-in-Water Emulsions.


Journal

Biomacromolecules
ISSN: 1526-4602
Titre abrégé: Biomacromolecules
Pays: United States
ID NLM: 100892849

Informations de publication

Date de publication:
08 02 2021
Historique:
pubmed: 21 1 2021
medline: 22 6 2021
entrez: 20 1 2021
Statut: ppublish

Résumé

Hydrophobically modified chitooligosaccharides (COSs) were tested for suitability as an emulsifier in cationic bituminous emulsions. COSs with polymerization degrees (DPs) of 5, 10, 15, and 20 were obtained by nitrous acid deamination. A complete study on depolymerization and precise product and side product characterization was undergone. Chemical modification of COSs was performed to achieve amphiphilic structures using three fatty epoxides with a growing chain length butyl (C4), octadecyl (C9), and hexadecyl glycidyl ether (C16)). The grafting efficiency according to reaction conditions was established. Different substitution degrees (DSs) were obtained by modulating the ratio of fatty epoxy to NH

Identifiants

pubmed: 33470101
doi: 10.1021/acs.biomac.0c01576
doi:

Substances chimiques

Emulsions 0
Epoxy Compounds 0
Phenols 0
Water 059QF0KO0R
cardanol 4TB1UYZ2LN
Chitosan 9012-76-4

Types de publication

Journal Article Research Support, Non-U.S. Gov't

Langues

eng

Sous-ensembles de citation

IM

Pagination

846-854

Auteurs

Camille Chapelle (C)

ICGM, Univ Montpellier, CNRS, ENSCM, Montpellier 3090, France.

Ghislain David (G)

ICGM, Univ Montpellier, CNRS, ENSCM, Montpellier 3090, France.

Sylvain Caillol (S)

ICGM, Univ Montpellier, CNRS, ENSCM, Montpellier 3090, France.

Claire Negrell (C)

ICGM, Univ Montpellier, CNRS, ENSCM, Montpellier 3090, France.

Graziella Durand (G)

CST COLAS 4, Rue Jean Mermoz CS 30504, Magny-les-Hameaux Cedex 78771, France.

Myriam Desroches le Foll (MD)

CST COLAS 4, Rue Jean Mermoz CS 30504, Magny-les-Hameaux Cedex 78771, France.

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Classifications MeSH