Lipopolysaccharide from Gut-Associated Lymphoid-Tissue-Resident Alcaligenes faecalis: Complete Structure Determination and Chemical Synthesis of Its Lipid A.


Journal

Angewandte Chemie (International ed. in English)
ISSN: 1521-3773
Titre abrégé: Angew Chem Int Ed Engl
Pays: Germany
ID NLM: 0370543

Informations de publication

Date de publication:
26 04 2021
Historique:
received: 10 09 2020
pubmed: 2 2 2021
medline: 7 8 2021
entrez: 1 2 2021
Statut: ppublish

Résumé

Alcaligenes faecalis is the predominant Gram-negative bacterium inhabiting gut-associated lymphoid tissues, Peyer's patches. We previously reported that an A. faecalis lipopolysaccharide (LPS) acted as a weak agonist for Toll-like receptor 4 (TLR4)/myeloid differentiation factor-2 (MD-2) receptor as well as a potent inducer of IgA without excessive inflammation, thus suggesting that A. faecalis LPS might be used as a safe adjuvant. In this study, we characterized the structure of both the lipooligosaccharide (LOS) and LPS from A. faecalis. We synthesized three lipid A molecules with different degrees of acylation by an efficient route involving the simultaneous introduction of 1- and 4'-phosphates. Hexaacylated A. faecalis lipid A showed moderate agonistic activity towards TLR4-mediated signaling and the ability to elicit a discrete interleukin-6 release in human cell lines and mice. It was thus found to be the active principle of the LOS/LPS and a promising vaccine adjuvant candidate.

Identifiants

pubmed: 33522128
doi: 10.1002/anie.202012374
pmc: PMC8252424
doi:

Substances chimiques

Interleukin-6 0
Lipid A 0
Lipopolysaccharides 0
TLR4 protein, human 0
Tlr4 protein, mouse 0
Toll-Like Receptor 4 0

Types de publication

Journal Article Research Support, Non-U.S. Gov't

Langues

eng

Sous-ensembles de citation

IM

Pagination

10023-10031

Informations de copyright

© 2021 The Authors. Angewandte Chemie International Edition published by Wiley-VCH GmbH.

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Auteurs

Atsushi Shimoyama (A)

Department of Chemistry, Graduate School of Science, Osaka University, 1-1 Machikaneyama, Toyonaka, Osaka, 560-0043, Japan.
Project Research Center for Fundamental Sciences, Osaka University, 1-1 Machikaneyama, Toyonaka, Osaka, 560-0043, Japan.

Flaviana Di Lorenzo (F)

Department of Chemical Sciences and Task Force on Microbiome Studies, University of Naples Federico II, Via Cinthia 4, 80126, Naples, Italy.

Haruki Yamaura (H)

Department of Chemistry, Graduate School of Science, Osaka University, 1-1 Machikaneyama, Toyonaka, Osaka, 560-0043, Japan.

Keisuke Mizote (K)

Department of Chemistry, Graduate School of Science, Osaka University, 1-1 Machikaneyama, Toyonaka, Osaka, 560-0043, Japan.

Angelo Palmigiano (A)

CNR, Institute for Polymers, Composites and Biomaterials IPCB, Via P. Gaifami 18, 95126, Catania, Italy.

Molly D Pither (MD)

Department of Chemical Sciences, University of Naples Federico II, Via Cinthia 4, 80126, Naples, Italy.

Immacolata Speciale (I)

Department of Chemical Sciences and Task Force on Microbiome Studies, University of Naples Federico II, Via Cinthia 4, 80126, Naples, Italy.

Tomoya Uto (T)

Department of Chemistry, Graduate School of Science, Osaka University, 1-1 Machikaneyama, Toyonaka, Osaka, 560-0043, Japan.

Seiji Masui (S)

Department of Chemistry, Graduate School of Science, Osaka University, 1-1 Machikaneyama, Toyonaka, Osaka, 560-0043, Japan.

Luisa Sturiale (L)

CNR, Institute for Polymers, Composites and Biomaterials IPCB, Via P. Gaifami 18, 95126, Catania, Italy.

Domenico Garozzo (D)

CNR, Institute for Polymers, Composites and Biomaterials IPCB, Via P. Gaifami 18, 95126, Catania, Italy.

Koji Hosomi (K)

Laboratory of Vaccine Materials, Center for Vaccine and Adjuvant Research, and Laboratory of Gut Environmental System, National Institutes of Biomedical Innovation, Health and Nutrition, Osaka, 567-0085, Japan.

Naoko Shibata (N)

Faculty of Science and Engineering, Waseda University, 3-4-1 Okubo, Shinjuku-ku, Tokyo, 169-8555, Japan.

Kazuya Kabayama (K)

Department of Chemistry, Graduate School of Science, Osaka University, 1-1 Machikaneyama, Toyonaka, Osaka, 560-0043, Japan.
Project Research Center for Fundamental Sciences, Osaka University, 1-1 Machikaneyama, Toyonaka, Osaka, 560-0043, Japan.

Yukari Fujimoto (Y)

Faculty of Science and Technology, Keio University, 3-14-1 Hiyoshi, Kohoku-ku, Yokohama, Kanagawa, 223-8522, Japan.

Alba Silipo (A)

Department of Chemical Sciences and Task Force on Microbiome Studies, University of Naples Federico II, Via Cinthia 4, 80126, Naples, Italy.

Jun Kunisawa (J)

Laboratory of Vaccine Materials, Center for Vaccine and Adjuvant Research, and Laboratory of Gut Environmental System, National Institutes of Biomedical Innovation, Health and Nutrition, Osaka, 567-0085, Japan.
International Research and Development Center for Mucosal Vaccines, The Institute of Medical Science, The University of Tokyo, 4-6-1 Shirokanedai, Minato-ku, Tokyo, 108-8639, Japan.

Hiroshi Kiyono (H)

International Research and Development Center for Mucosal Vaccines, The Institute of Medical Science, The University of Tokyo, 4-6-1 Shirokanedai, Minato-ku, Tokyo, 108-8639, Japan.

Antonio Molinaro (A)

Department of Chemistry, Graduate School of Science, Osaka University, 1-1 Machikaneyama, Toyonaka, Osaka, 560-0043, Japan.
Department of Chemical Sciences and Task Force on Microbiome Studies, University of Naples Federico II, Via Cinthia 4, 80126, Naples, Italy.

Koichi Fukase (K)

Department of Chemistry, Graduate School of Science, Osaka University, 1-1 Machikaneyama, Toyonaka, Osaka, 560-0043, Japan.
Project Research Center for Fundamental Sciences, Osaka University, 1-1 Machikaneyama, Toyonaka, Osaka, 560-0043, Japan.

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Classifications MeSH