Self-Diagnostic Polymers-Inline Detection of Thermal Degradation of Unsaturated Poly(ester imide)s.
chemosensors
optical sensors
poly(ester imide)s
stilbenes
thermal polymer degradation
Journal
Advanced materials (Deerfield Beach, Fla.)
ISSN: 1521-4095
Titre abrégé: Adv Mater
Pays: Germany
ID NLM: 9885358
Informations de publication
Date de publication:
May 2021
May 2021
Historique:
revised:
02
02
2021
received:
05
01
2021
pubmed:
31
3
2021
medline:
31
3
2021
entrez:
30
3
2021
Statut:
ppublish
Résumé
Monitoring polymer degradation is an important quest, particularly relevant for industry. Although many indirect methodologies for assessing polymer degradation exist, only few are applicable for an inline-monitoring via optic detection-systems. An inline-monitoring system is introduced for the thermal degradation of crosslinked poly(ester imide)s (PEIs) by embedding trifluoroacetyl functionalized stilbene molecules, serving as chemosensors to track the release of generated alcoholic byproducts. Nucleophilic addition of an alcohol to the sensors trifluoroacetyl functionality triggers hemiacetal formation which is accompanied by significant changes in optical properties, in turn allowing monitoring of sensor activation by direct spectroscopy. Fluorescence spectroscopy offers an easy detection tool for the inline thermal monitoring of PEI-degradation.
Identifiants
pubmed: 33783026
doi: 10.1002/adma.202100068
doi:
Types de publication
Journal Article
Langues
eng
Sous-ensembles de citation
IM
Pagination
e2100068Subventions
Organisme : ALTANA AG
Organisme : EU-BAT-4-ever project
ID : EU-HORIZON 2020
Informations de copyright
© 2021 The Authors. Advanced Materials published by Wiley-VCH GmbH.
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