New Sustainable, Scalable and One-Step Synthesis of Iron Oxide Nanoparticles by Ion Exchange Process.

ferrihydrite nanoparticles hematite nanoparticles ion exchange process magnetite nanoparticles δ-FeOOH nanoparticles

Journal

Nanomaterials (Basel, Switzerland)
ISSN: 2079-4991
Titre abrégé: Nanomaterials (Basel)
Pays: Switzerland
ID NLM: 101610216

Informations de publication

Date de publication:
20 Mar 2021
Historique:
received: 21 02 2021
revised: 08 03 2021
accepted: 17 03 2021
entrez: 3 4 2021
pubmed: 4 4 2021
medline: 4 4 2021
Statut: epublish

Résumé

This work introduces an innovative, sustainable, and scalable synthesis of iron oxides nanoparticles (NPs) in aqueous suspension. The method, based on ion exchange process, consists of a one-step procedure, time and energy saving, operating in water and at room temperature, by cheap and renewable reagents. The influence of both oxidation state of the initial reagent and reaction atmosphere is considered. Three kinds of iron nanostructured compounds are obtained (2-lines ferrihydrite; layered-structure iron oxyhydroxide δ-FeOOH; and cubic magnetite), in turn used as precursors to obtain hematite and maghemite NPs. All the produced NPs are characterized by a high purity, small particles dimensions (from 2 to 50 nm), and high specific surface area values up to 420 m

Identifiants

pubmed: 33804704
pii: nano11030798
doi: 10.3390/nano11030798
pmc: PMC8004010
pii:
doi:

Types de publication

Journal Article

Langues

eng

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Auteurs

Ludovico Macera (L)

Department of Industrial and Information Engineering and Economics, University of L'Aquila, Piazzale E. Pontieri 1, Monteluco di Roio, I-67100 L'Aquila, Italy.

Valeria Daniele (V)

Department of Industrial and Information Engineering and Economics, University of L'Aquila, Piazzale E. Pontieri 1, Monteluco di Roio, I-67100 L'Aquila, Italy.

Claudia Mondelli (C)

CNR-IOM-OGG, Institut Laue Langevin, 71 Avenue des Martyrs, CEDEX 9, 38042 Grenoble, France.

Marie Capron (M)

ESRF-The European Synchrotron, 71 Avenue des Martyrs, CEDEX 9, 38042 Grenoble, France.
Partnership for Soft Condensed Matter (PSCM), ESRF-The European Synchrotron, 71 Avenue des Martyrs, CEDEX 9, 38042 Grenoble, France.

Giuliana Taglieri (G)

Department of Industrial and Information Engineering and Economics, University of L'Aquila, Piazzale E. Pontieri 1, Monteluco di Roio, I-67100 L'Aquila, Italy.

Classifications MeSH