Direct measurement of pregnanediol 3-glucuronide (PDG) in dried urine spots by liquid chromatography-mass spectrometry to detect ovulation.


Journal

The Journal of steroid biochemistry and molecular biology
ISSN: 1879-1220
Titre abrégé: J Steroid Biochem Mol Biol
Pays: England
ID NLM: 9015483

Informations de publication

Date de publication:
07 2021
Historique:
received: 18 02 2021
revised: 17 03 2021
accepted: 07 04 2021
pubmed: 20 4 2021
medline: 31 8 2021
entrez: 19 4 2021
Statut: ppublish

Résumé

Non-invasive self-testing using an objective chemical method to detect ovulation is valuable for women planning conception, practising contraception or undergoing infertility investigations or treatment. Based on luteal phase secretion of progesterone (P Urine PDG with and without creatinine adjustment was stable during the follicular phase with the expected striking rise in the luteal phase peaking at 5 days after ovulation. Using a single spot urine sample (100 μL) or a DUS (<20 μL urine) and an optimal threshold to distinguish pre- from post-ovulatory samples, in ROC analysis urine PDG adjusted for creatinine accurately identified ovulation in 92 % of samples was comparable with P3G immunoassay and superior to urine P This method holds promise as a non-invasive self-test method for women to determine by an objective chemical method their ovulatory status.

Sections du résumé

BACKGROUND
Non-invasive self-testing using an objective chemical method to detect ovulation is valuable for women planning conception, practising contraception or undergoing infertility investigations or treatment.
METHODS
Based on luteal phase secretion of progesterone (P
RESULTS
Urine PDG with and without creatinine adjustment was stable during the follicular phase with the expected striking rise in the luteal phase peaking at 5 days after ovulation. Using a single spot urine sample (100 μL) or a DUS (<20 μL urine) and an optimal threshold to distinguish pre- from post-ovulatory samples, in ROC analysis urine PDG adjusted for creatinine accurately identified ovulation in 92 % of samples was comparable with P3G immunoassay and superior to urine P
CONCLUSIONS
This method holds promise as a non-invasive self-test method for women to determine by an objective chemical method their ovulatory status.

Identifiants

pubmed: 33872762
pii: S0960-0760(21)00093-5
doi: 10.1016/j.jsbmb.2021.105900
pii:
doi:

Substances chimiques

Biomarkers 0
pregnanediol-3 alpha-glucuronide 1852-49-9
Pregnanediol JR3JD1Y22C

Types de publication

Journal Article Research Support, Non-U.S. Gov't

Langues

eng

Sous-ensembles de citation

IM

Pagination

105900

Subventions

Organisme : Medical Research Council
ID : MR/N022556/1
Pays : United Kingdom
Organisme : Wellcome Trust
ID : MR/N022556/1
Pays : United Kingdom
Organisme : Wellcome Trust
ID : 102419/Z/13/A
Pays : United Kingdom

Informations de copyright

Crown Copyright © 2021. Published by Elsevier Ltd. All rights reserved.

Auteurs

David J Handelsman (DJ)

Andrology laboratory, ANZAC Research Institute, University of Sydney, Concord Hospital, NSW, 2139, Australia. Electronic address: djh@anzac.edu.au.

Rama Nimmagadda (R)

Andrology laboratory, ANZAC Research Institute, University of Sydney, Concord Hospital, NSW, 2139, Australia.

Reena Desai (R)

Andrology laboratory, ANZAC Research Institute, University of Sydney, Concord Hospital, NSW, 2139, Australia.

Timothy D Handelsman (TD)

Andrology laboratory, ANZAC Research Institute, University of Sydney, Concord Hospital, NSW, 2139, Australia.

Belinda Whittle (B)

MyHealthTest Pty Ltd, Canberra, ACT, Australia.

Karolina Skorupskaite (K)

MRC Centre for Reproductive Health, Queens Medical Research Institute, University of Edinburgh, Scotland, UK.

Richard A Anderson (RA)

MRC Centre for Reproductive Health, Queens Medical Research Institute, University of Edinburgh, Scotland, UK.

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Classifications MeSH