Novel experimental setup for megahertz X-ray diffraction in a diamond anvil cell at the High Energy Density (HED) instrument of the European X-ray Free-Electron Laser (EuXFEL).

X-ray free-electron lasers diamond anvil cells finite element modeling high-precision X-ray diffraction

Journal

Journal of synchrotron radiation
ISSN: 1600-5775
Titre abrégé: J Synchrotron Radiat
Pays: United States
ID NLM: 9888878

Informations de publication

Date de publication:
01 May 2021
Historique:
received: 19 10 2020
accepted: 08 03 2021
entrez: 5 5 2021
pubmed: 6 5 2021
medline: 6 5 2021
Statut: ppublish

Résumé

The high-precision X-ray diffraction setup for work with diamond anvil cells (DACs) in interaction chamber 2 (IC2) of the High Energy Density instrument of the European X-ray Free-Electron Laser is described. This includes beamline optics, sample positioning and detector systems located in the multipurpose vacuum chamber. Concepts for pump-probe X-ray diffraction experiments in the DAC are described and their implementation demonstrated during the First User Community Assisted Commissioning experiment. X-ray heating and diffraction of Bi under pressure, obtained using 20 fs X-ray pulses at 17.8 keV and 2.2 MHz repetition, is illustrated through splitting of diffraction peaks, and interpreted employing finite element modeling of the sample chamber in the DAC.

Identifiants

DOI: 10.1107/S1600577521002551 PMID: 33949979 PMC: PMC8127375
pubmed: 33949979
pii: S1600577521002551
doi: 10.1107/S1600577521002551
pmc: PMC8127375
doi:

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

688-706

Subventions

Organisme : Horizon 2020 Framework Programme
ID : 730872
Organisme : Horizon 2020 Framework Programme
ID : 670787
Organisme : Horizon 2020 Framework Programme
ID : 864877
Organisme : Deutsche Forschungsgemeinschaft
ID : FOR 2440
Organisme : Ministry of Science, ICT and Future Planning
ID : NRF-2018R1A3B1052042
Organisme : U.S. Department of Energy
ID : DE-AC52-07 N A27344
Organisme : U.S. Department of Energy
ID : 89233218CNA000001
Organisme : U.S. Department of Energy
ID : 20190643DR
Organisme : U.S. Department of Energy
ID : DE-AC02-76SF00515
Organisme : U.S. Department of Energy
ID : FWP100182
Organisme : Engineering and Physical Sciences Research Council
ID : EP/P024513/1
Organisme : Engineering and Physical Sciences Research Council
ID : EP/R02927X/1
Organisme : U.S. Department of Energy, National Nuclear Security Administration
ID : DE-NA0003342
Organisme : National Science Foundation
ID : DMR-1701360
Organisme : Army Research Office
ID : W911NF-17-1-0468
Organisme : Army Research Office
ID : W911NF-19-2-0172
Organisme : National Science Foundation - Earth Sciences
ID : EAR-1634415

Informations de copyright

open access.

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Auteurs

H P Liermann (HP)

Photon Sciences, Deutsches Elektronen-Synchrotron (DESY), Notkestraße 85, Hamburg, Germany.
ORCID: 0000-0001-5039-1183

Z Konôpková (Z)

European X-Ray Free-Electron Laser Facility GmbH, Holzkoppel 4, 22869 Schenefeld, Germany.

K Appel (K)

European X-Ray Free-Electron Laser Facility GmbH, Holzkoppel 4, 22869 Schenefeld, Germany.

C Prescher (C)

Photon Sciences, Deutsches Elektronen-Synchrotron (DESY), Notkestraße 85, Hamburg, Germany.

A Schropp (A)

Photon Sciences, Deutsches Elektronen-Synchrotron (DESY), Notkestraße 85, Hamburg, Germany.

V Cerantola (V)

European X-Ray Free-Electron Laser Facility GmbH, Holzkoppel 4, 22869 Schenefeld, Germany.

R J Husband (RJ)

Photon Sciences, Deutsches Elektronen-Synchrotron (DESY), Notkestraße 85, Hamburg, Germany.

J D McHardy (JD)

School of Physics and Astronomy, Centre for Science at Extreme Conditions, and SUPA, University of Edinburgh, Peter Guthrie Tait Road, Edinburgh EH9 3FD, United Kingdom.

M I McMahon (MI)

School of Physics and Astronomy, Centre for Science at Extreme Conditions, and SUPA, University of Edinburgh, Peter Guthrie Tait Road, Edinburgh EH9 3FD, United Kingdom.

R S McWilliams (RS)

School of Physics and Astronomy, Centre for Science at Extreme Conditions, and SUPA, University of Edinburgh, Peter Guthrie Tait Road, Edinburgh EH9 3FD, United Kingdom.

C M Pépin (CM)

CEA, DAM, DIF, F-91297 Arpajon, France.

J Mainberger (J)

Photon Sciences, Deutsches Elektronen-Synchrotron (DESY), Notkestraße 85, Hamburg, Germany.

M Roeper (M)

Photon Sciences, Deutsches Elektronen-Synchrotron (DESY), Notkestraße 85, Hamburg, Germany.

A Berghäuser (A)

Helmholtz Zentrum Dresden Rossendorf e.V., 01328 Dresden, Germany.

H Damker (H)

Photon Sciences, Deutsches Elektronen-Synchrotron (DESY), Notkestraße 85, Hamburg, Germany.

P Talkovski (P)

Photon Sciences, Deutsches Elektronen-Synchrotron (DESY), Notkestraße 85, Hamburg, Germany.

M Foese (M)

Photon Sciences, Deutsches Elektronen-Synchrotron (DESY), Notkestraße 85, Hamburg, Germany.

N Kujala (N)

European X-Ray Free-Electron Laser Facility GmbH, Holzkoppel 4, 22869 Schenefeld, Germany.

O B Ball (OB)

School of Physics and Astronomy, Centre for Science at Extreme Conditions, and SUPA, University of Edinburgh, Peter Guthrie Tait Road, Edinburgh EH9 3FD, United Kingdom.

M A Baron (MA)

Institut de Minéralogie, de Physique des Matériaux et de Cosmochimie (IMPMC), Sorbonne Université, UMR CNRS 7590, Musée National d'Histoire Naturelle, 4 Place Jussieu, Paris, France.

R Briggs (R)

Lawrence Livermore National Laboratory, 7000 East Avenue, Livermore, CA 94550, USA.

M Bykov (M)

Carnegie Science, Earth and Planets Laboratory, 5241 Broad Branch Road NW, Washington, DC 20015, USA.

E Bykova (E)

Carnegie Science, Earth and Planets Laboratory, 5241 Broad Branch Road NW, Washington, DC 20015, USA.

J Chantel (J)

Université de Lille, CNRS, INRAE, Centrale Lille, UMR 8207 - UMET - Unité Matériaux et Transformations, F-59000 Lille, France.

A L Coleman (AL)

Lawrence Livermore National Laboratory, 7000 East Avenue, Livermore, CA 94550, USA.

H Cynn (H)

Lawrence Livermore National Laboratory, 7000 East Avenue, Livermore, CA 94550, USA.

D Dattelbaum (D)

Los Alamos National Laboratory, Los Alamos, NM 87545, USA.

L E Dresselhaus-Marais (LE)

Lawrence Livermore National Laboratory, 7000 East Avenue, Livermore, CA 94550, USA.

J H Eggert (JH)

Lawrence Livermore National Laboratory, 7000 East Avenue, Livermore, CA 94550, USA.

L Ehm (L)

Mineral Physics Institute, Stony Brook University, Stony Brook, NY 11794, USA.

W J Evans (WJ)

Lawrence Livermore National Laboratory, 7000 East Avenue, Livermore, CA 94550, USA.

G Fiquet (G)

Institut de Minéralogie, de Physique des Matériaux et de Cosmochimie (IMPMC), Sorbonne Université, UMR CNRS 7590, Musée National d'Histoire Naturelle, 4 Place Jussieu, Paris, France.

M Frost (M)

SLAC National Accelerator Laboratory, 2575 Sand Hill Road, Menlo Park, CA 94025, USA.

K Glazyrin (K)

Photon Sciences, Deutsches Elektronen-Synchrotron (DESY), Notkestraße 85, Hamburg, Germany.

A F Goncharov (AF)

Carnegie Science, Earth and Planets Laboratory, 5241 Broad Branch Road NW, Washington, DC 20015, USA.

H Hwang (H)

Department of Earth System Sciences, Yonsei University, 50 Yonsei-ro, Seodaemun-gu, Seoul 03722, Republic of Korea.

Zs Jenei (Z)

Lawrence Livermore National Laboratory, 7000 East Avenue, Livermore, CA 94550, USA.
ORCID: 0000-0003-4347-1251

J Y Kim (JY)

Department of Physics, Research Institute for High Pressure, Hanyang University, 222 Wangsimni-ro, Seoul 04763, Republic of Korea.

F Langenhorst (F)

Institute of Geosciences, Friedrich Schiller University Jena, Carl-Zeiss-Promenade 10, 07745 Jena, Germany.

Y Lee (Y)

Department of Earth System Sciences, Yonsei University, 50 Yonsei-ro, Seodaemun-gu, Seoul 03722, Republic of Korea.

M Makita (M)

European X-Ray Free-Electron Laser Facility GmbH, Holzkoppel 4, 22869 Schenefeld, Germany.

H Marquardt (H)

Department of Earth Sciences, University of Oxford, South Parks Road, Oxford OX1 3AN, United Kingdom.

E E McBride (EE)

SLAC National Accelerator Laboratory, 2575 Sand Hill Road, Menlo Park, CA 94025, USA.

S Merkel (S)

Université de Lille, CNRS, INRAE, Centrale Lille, UMR 8207 - UMET - Unité Matériaux et Transformations, F-59000 Lille, France.

G Morard (G)

Institut de Minéralogie, de Physique des Matériaux et de Cosmochimie (IMPMC), Sorbonne Université, UMR CNRS 7590, Musée National d'Histoire Naturelle, 4 Place Jussieu, Paris, France.

E F O'Bannon (EF)

Lawrence Livermore National Laboratory, 7000 East Avenue, Livermore, CA 94550, USA.

C Otzen (C)

Photon Sciences, Deutsches Elektronen-Synchrotron (DESY), Notkestraße 85, Hamburg, Germany.

E J Pace (EJ)

School of Physics and Astronomy, Centre for Science at Extreme Conditions, and SUPA, University of Edinburgh, Peter Guthrie Tait Road, Edinburgh EH9 3FD, United Kingdom.

A Pelka (A)

Helmholtz Zentrum Dresden Rossendorf e.V., 01328 Dresden, Germany.

J S Pigott (JS)

Los Alamos National Laboratory, Los Alamos, NM 87545, USA.

V B Prakapenka (VB)

Center for Advanced Radiation Sources, University of Chicago, Chicago, IL 60637, USA.
ORCID: 0000-0001-9270-2330

R Redmer (R)

Institut für Physik, Universität Rostock, D-18051 Rostock, Germany.

C Sanchez-Valle (C)

Institut für Mineralogie, University of Münster, Münster, Germany.

M Schoelmerich (M)

European X-Ray Free-Electron Laser Facility GmbH, Holzkoppel 4, 22869 Schenefeld, Germany.

S Speziale (S)

GFZ German Research Centre for Geosciences, Telegrafenberg, 14473 Potsdam, Germany.

G Spiekermann (G)

Institut für Geowissenschaften, Universität Potsdam, Karl-Liebknecht-Straße 24-25, 14476 Potsdam, Germany.

B T Sturtevant (BT)

Los Alamos National Laboratory, Los Alamos, NM 87545, USA.

S Toleikis (S)

Photon Sciences, Deutsches Elektronen-Synchrotron (DESY), Notkestraße 85, Hamburg, Germany.

N Velisavljevic (N)

Lawrence Livermore National Laboratory, 7000 East Avenue, Livermore, CA 94550, USA.

M Wilke (M)

Institut für Geowissenschaften, Universität Potsdam, Karl-Liebknecht-Straße 24-25, 14476 Potsdam, Germany.

C S Yoo (CS)

Department of Chemistry, Institute of Shock Physics, and Materials Science and Engineering, Washington State University, Pullman, WA 99164, USA.

C Baehtz (C)

Helmholtz Zentrum Dresden Rossendorf e.V., 01328 Dresden, Germany.

U Zastrau (U)

European X-Ray Free-Electron Laser Facility GmbH, Holzkoppel 4, 22869 Schenefeld, Germany.

C Strohm (C)

Photon Sciences, Deutsches Elektronen-Synchrotron (DESY), Notkestraße 85, Hamburg, Germany.

Classifications MeSH