Crosslinked Polydicyclopentadiene Nanoparticles via Ring-Opening Metathesis Polymerization-Induced Self-Assembly Approach.
crosslinked nanoparticles
polymerization-driven self-assembly
ring-opening metathesis polymerization
Journal
Macromolecular rapid communications
ISSN: 1521-3927
Titre abrégé: Macromol Rapid Commun
Pays: Germany
ID NLM: 9888239
Informations de publication
Date de publication:
Jul 2021
Jul 2021
Historique:
revised:
21
04
2021
received:
10
03
2021
pubmed:
1
6
2021
medline:
27
7
2021
entrez:
31
5
2021
Statut:
ppublish
Résumé
In this communication, the preparation of crosslinked polydicyclopentadiene (PDCPD) nanoparticles via ring-opening metathesis polymerization (ROMP)-induced self-assembly approach is reported. For the ROMPs, the macromolecular chain transfer agents (Macro-CTAs) are synthesized via the ring-opening polymerization (ROP) of ε-caprolactone (CL) with cis-2-butene-1,4-diol as the initiator. The ROMPs are performed with chloroform, tetrahydrofuran, toluene, 1,4-dioxane, and N,N-dimethylacetamide as the solvents, respectively, which are catalyzed with Grubbs second generation catalyst. It is found that the crosslinked PDCPD nanoparticles are obtained with spherical, cylindrical to planar morphologies, depending on the molecular weights of Macro-CTAs, the concentrations of DCPD and the natures of solvents. The polymerization induced self-assembly (ROMPISA) by the use of a non-norbornene-based macromolecular chain transfer agent provides a new and efficient approach to prepare crosslinked polymer nanoparticles.
Identifiants
pubmed: 34057258
doi: 10.1002/marc.202100155
doi:
Substances chimiques
Polymers
0
Types de publication
Journal Article
Langues
eng
Sous-ensembles de citation
IM
Pagination
e2100155Subventions
Organisme : National Natural Science Foundation of China
ID : 51973113
Organisme : National Natural Science Foundation of China
ID : 51133003
Organisme : National Natural Science Foundation of China
ID : 21774078
Informations de copyright
© 2021 Wiley-VCH GmbH.
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