Detection of Antimicrobial Residues in Poultry Litter: Monitoring a Risk through a Selective and Sensitive HPLC-MS/MS Method.
HPLC–MS/MS
agriculture fertilizer
antimicrobials
poultry litter
validation
Journal
Animals : an open access journal from MDPI
ISSN: 2076-2615
Titre abrégé: Animals (Basel)
Pays: Switzerland
ID NLM: 101635614
Informations de publication
Date de publication:
14 May 2021
14 May 2021
Historique:
received:
31
03
2021
revised:
18
04
2021
accepted:
19
04
2021
entrez:
2
6
2021
pubmed:
3
6
2021
medline:
3
6
2021
Statut:
epublish
Résumé
Tetracyclines, sulphonamides, and quinolones are families of antimicrobials (AMs) widely used in the poultry industry and can excrete up to 90% of AMs administrated, which accumulate in poultry litter. Worryingly, poultry litter is widely used as an agriculture fertilizer, contributing to the spread AMs residues in the environment. The aim of this research was to develop a method that could simultaneously identify and quantify three AMs families in poultry litter by high-performance liquid chromatography-tandem mass spectrometry (HPLC-MS/MS). Samples of AMs free poultry litter were used to validate the method according to 657/2002/EC and VICH GL49. Results indicate that limit of detection (LOD) ranged from 8.95 to 20.86 μg kg
Identifiants
pubmed: 34069030
pii: ani11051399
doi: 10.3390/ani11051399
pmc: PMC8156041
pii:
doi:
Types de publication
Journal Article
Langues
eng
Subventions
Organisme : Vicerrectoría de Investigación y Desarrollo (VID)
ID : VID2019 ENL07/19
Organisme : International Atomic Energy Agency
ID : Research contract 22180 (D52041)
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